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Preparation method of wetting agent for E glass fishing rod gauze

A technology of sizing and glass, applied in the field of preparation of E glass fiber surface treatment agent, can solve the problems of resin impermeability, loss of strength of fishing rod cloth, affecting the strength of fishing rod products, etc., to reduce energy consumption, low adhesion rate, The effect of improving the quality of the fishing rod

Active Publication Date: 2013-12-25
陕西汇友友基新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] The glass fiber fishing rod yarn produced by the paraffin-containing sizing agent has two disadvantages: a. It is not impregnated with epoxy resin, unsaturated resin, phenolic resin and other resins; b. Smoldering at ℃ for 24h-30h to dewax the sizing agent on the fiber surface
After dewaxing, the strength of the fishing rod cloth loses 20-40%, which directly affects the strength of the fishing rod product

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Preparation method of wetting agent for E glass fishing rod gauze
  • Preparation method of wetting agent for E glass fishing rod gauze
  • Preparation method of wetting agent for E glass fishing rod gauze

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0047] a. Take 9 kg of deionized water, add 0.05 kg of citric acid to adjust the Ph value to 3-4, slowly add 0.3 kg of silane coupling agent A-174 (GE Silicones, USA) while stirring, at 60-80rpm Stir for 30-60min;

[0048] b. Mix 0.02kg of plasticizer phthalic acid and 0.4kg of emulsifier Pingpingjia-20, then heat and melt at 80-95℃, and then add 8.4kg of 70-90 evenly within 30min-60min with stirring ℃ deionized water, the stirring speed is 1000rpm-3000rpm; then cool to below 30℃;

[0049] c. Add 1 kg of 80-90°C deionized water to 0.1 kg of imidazoline cationic lubricant ZB09 (produced by Xi'an Zhongchuang Composite Materials Co., Ltd.), and stir to form a uniform transparent liquid;

[0050] d. Add 0.36 kg of 30-50°C deionized water to 0.05 kg of antistatic agent 6660A (EMERY, USA), and stir to form a uniform transparent liquid;

[0051] e. Add 5 kg of deionized water to 1.0 kg of epoxy emulsion film-forming agent YG101 (produced by Xi'an Youji Composite Materials Co., L...

Embodiment 2

[0057] a. Take 10.5 kg of deionized water, add 0.05 kg of citric acid to adjust the Ph value to 3-4, slowly add 0.35 kg of silane coupling agent A-174 (GE Silicones, USA) while stirring, at 60-80rpm Stir for 30-60min;

[0058] b. Mix 0.04 kg of plasticizer dibutyl phthalate and 0.6 kg of emulsifier Pingpingjia-20, then heat and melt at 80-95 ° C, and then add 12.8 kg of 70-90°C deionized water, the stirring speed is 1000rpm-3000rpm; then cool to below 30°C;

[0059] c. Add 2.25 kg of 80-90°C deionized water to 0.15 kg of imidazoline cationic lubricant ZB09 (produced by Xi'an Zhongchuang Composite Materials Co., Ltd.), and stir to form a uniform transparent liquid;

[0060]d. Add 0.64 kg of 30-50°C deionized water to 0.08 kg of antistatic agent 6660A (EMERY, USA), and stir to form a uniform transparent liquid;

[0061] e. Add 10 kg of deionized water to 2.0 kg of epoxy emulsion film-forming agent YG101 (produced by Xi'an Youji Composite Materials Co., Ltd.);

[0062] Add ...

Embodiment 3

[0067] a. Take 12 kg of deionized water, add 0.06 kg of citric acid to adjust the Ph value to 3-4, slowly add 0.2 kg of silane coupling agent A-174 (GE Silicones, USA) and 0.2 kg of silane coupling agent while stirring Agent A-1100 (GE Silicones, USA), stirred for 30-60min under the condition of 60-80rpm;

[0068] b. Mix 0.04kg of plasticizer dibutyl phthalate and 0.6kg of emulsifier Pingpingjia-20, then heat and melt at 80-95℃, and then add 12.8kg of 70-90°C deionized water, the stirring speed is 1000rpm-3000rpm; then cool to below 30°C;

[0069] c. Add 2.25 kg of 80-90°C deionized water to 0.15 kg of imidazoline cationic lubricant ZB09 (produced by Xi'an Zhongchuang Composite Materials Co., Ltd.), and stir to form a uniform transparent liquid;

[0070] d. Add 1 kg of 30-50°C deionized water to 0.1 kg of antistatic agent 6660A (EMERY, USA), and stir to form a uniform transparent liquid;

[0071] e. Add 12.5 kg of deionized water to 3.0 kg of epoxy emulsion film-forming a...

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Abstract

The invention relates to a preparation method of an organic-material-containing E glass fiber surface treating agent. The preparation method comprises the following steps: adding citric acid into deionized water to regulate the pH value to 3-4, slowly adding a silane coupling agent, and stirring at 60-80 rpm for 30-60 minutes; mixing a plasticizer and an emulsifier, melting by heating, and uniformly adding 5-20 times by weight of 70-90 DEG C deionized water within 30-60 minutes while stirring; cooling to 30 DEG C below; adding 80-90 DEG C deionized water into an imidazoline cation lubricant, and stirring uniformly to obtain a transparent solution; adding 30-50 DEG C deionized water into an antistatic agent, and stirring uniformly to obtain a transparent solution; respectively adding 1-5 times by mass of deionized water into an epoxy emulsion film former and an unsaturated polyester film former; and mixing all the substances prepared in all the steps above, adding deionized water, and stirring at 50-60 rpm for 30-40 minutes. The product can enable the E glass fiber fishing rod gauze to have high permeation speed and favorable binding property with epoxy resin, unsaturated polyester resin and phenol aldehyde resin.

Description

technical field [0001] The invention relates to a preparation method of an E glass fiber surface treatment agent containing organic materials. Background technique [0002] E glass fiber fishing rod cloth yarn is mainly used for weaving fishing rod cloth. Fishing rod cloth is a reinforced base material for the production of fishing rods. It requires good combination with epoxy resin, unsaturated resin, phenolic resin, etc. The sizing agent used in the production of traditional E glass fiber fishing rod yarn is made of paraffin wax, stearic acid, transformer oil, color fixing agent, leveling agent and emulsifier. Its components (wt%) are as follows: [0003] Engine oil: 0.5-3.0 [0004] Vaseline: 1.0-2.0 [0005] Paraffin: 1.5-2.5 [0006] Stearic acid: 2.0-4.0 [0007] Fixing agent: 2.0-6.0 [0008] Pingpinga 20:0.5-1.0 [0009] Deionized water: 81.5-94.5. [0010] The glass fiber fishing rod yarn produced by the paraffin-containing sizing agent has two disadvantages:...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C25/40
Inventor 任川荣张永海贾媛媛
Owner 陕西汇友友基新材料有限公司
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