Micro-emulsion viscosity reducer for thick oil, and preparation method thereof
An oil-soluble viscosity reducer and microemulsion technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problems of poor oil adaptability and high cost of use of surfactant-based viscosity reducers, and achieve product stability Good performance, improve the degree of uniform use, and strong adaptability
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Embodiment 1
[0026] The preparation method is carried out as follows:
[0027] a. Take 16 kilograms of OP-10 emulsifier and place it in the reactor, add 24 kilograms of tap water, and gradually heat up to 60°C under stirring conditions of 25 revolutions / min (the heating rate does not exceed 1°C / min);
[0028] b. Reduce the stirring rate to 10 revolutions / min, add 18 kg of anionic surfactant ABS sodium dodecylbenzene sulfonate to the reaction kettle of step a in 5 times, continue to stir for 25 minutes, and then slowly add 37 kg No. 120 solvent oil is added to ensure the air flow in the workshop, and fireworks are strictly prohibited.
[0029] c. Increase the stirring rate to 35 revolutions / min. Under stirring, add 2 kg of Tween 80 emulsifier and 5 kg of long-chain isomeric alcohol to the reaction kettle in turn, and stop heating;
[0030] d. After the reactor is naturally cooled to room temperature, stir for 10 minutes and then put it into the finished product container.
Embodiment 2
[0032] The preparation method is carried out as follows:
[0033] a. Take 20 kg of OP-10 emulsifier and place it in the reactor, add 20 kg of tap water, and gradually increase the temperature to 55°C under the condition of stirring at 35 revolutions / min (the heating rate does not exceed 1°C / min);
[0034] b. Reduce the stirring rate to 20 revolutions / min, add 22 kg of anionic surfactant ABS sodium dodecylbenzene sulfonate to the reactor of step a in 3 times, continue to stir for 40 minutes, and then slowly add 33 kg No. 120 solvent oil is added to ensure the air flow in the workshop, and fireworks are strictly prohibited.
[0035] c. Increase the stirring rate to 25 revolutions / min. Under stirring, add 4 kg of Tween 80 emulsifier and 3 kg of long-chain isomeric alcohol to the reaction kettle in turn, and stop heating;
[0036] d. After the reactor is naturally cooled to room temperature, it is stirred for 30 minutes and then filled into the finished product container.
Embodiment 3
[0038] The preparation method is carried out as follows:
[0039] a. Take 18 kilograms of OP-10 emulsifier and place it in the reactor, add 22 kilograms of tap water, and gradually heat up to 58°C under stirring conditions of 30 revolutions / min (the heating rate does not exceed 1°C / min);
[0040] b. Reduce the stirring rate to 15 revolutions / min, add 20 kg of anionic surfactant ABS sodium dodecylbenzene sulfonate to the reaction kettle of step a in 4 times, continue to stir for 30 minutes, and then slowly add 35 kg No. 120 solvent oil is added to ensure the air flow in the workshop, and fireworks are strictly prohibited.
[0041] c. Increase the stirring rate to 30 revolutions / min. Under stirring, add 3 kg of Tween 80 emulsifier and 4 kg of long-chain isomeric alcohol to the reaction kettle in turn, and stop heating;
[0042] d. After the reaction kettle is naturally cooled to room temperature, stir for 20 minutes and then put it into the finished product container.
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Abstract
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