Inkjet inks, microlenses, optical components and devices
A technology for inkjet inks and optical parts, applied in the field of inkjet inks, can solve the problems of increased production lead time, increased number of manufacturing steps, etc., and achieve the effect of good shape
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[0187] 1-8. Preparation method of ink
[0188] The ink of the present invention can be prepared by mixing the ingredients used as raw materials by a known method.
[0189] In particular, the ink of the present invention is preferably prepared by combining the (meth)acrylamide (A), cyclic (meth)acrylamide (B), and (meth)acrylic urethane (C) And a photoinitiator (D), and other components as needed are mixed, and the obtained solution is filtered and degassed, for example using a membrane filter (membrane filter). The ink prepared as described above has excellent ejection properties.
[0190] 1-9. Using inkjet method to apply ink
[0191] The ink of the present invention can be applied using a known inkjet method. Examples of the inkjet method include: a piezoelectric method in which mechanical energy is applied to the ink to eject the ink from an inkjet head, and a coating method in which thermal energy is applied to the ink to eject the ink (so-called thermal) the way).
[0192] By u...
Embodiment 1
[0224] Use HEAA (trade name; Koto Co., Ltd.) as N-(hydroxyethyl)acrylamide as (meth)acrylamide (A) and ACMO (trade name; Koto Co., Ltd. as N-acryloyl morphine) ) CN9893 as cyclic (meth)acrylamide (B) and (meth)acrylic urethane (C) (trade name; Sartomer Co., Ltd., bifunctional (meth)acrylic urethane) Ester), and as oxy-phenyl-acetic acid-2-[2-oxo-2-phenyl-acetoxy-ethoxy]-ethyl ester and oxy-phenyl-acetic acid-2-[2 -Hydroxy-ethoxy]-ethyl ester mixture of IRGACURE754 (trade name; BASF Corporation, hereinafter referred to as "Ir754") as the photopolymerization initiator (D), mixed in the following composition ratio, and completely dissolved After that, filtration was performed with a membrane filter (0.2 μm) made of ultra-high molecular weight polyethylene (UPE) to obtain a filtrate (ink 1).
[0225] (A)HEAA 10.00g
[0226] (B)ACMO 78.00g
[0227] (C)CN9893 12.00g
[0228] (D)Ir754 7.00g
[0229] Using an E-type viscometer (TV-22 of Toki Sangyo Co., Ltd., the same below), the viscosity ...
Embodiment 2
[0231] KAYARAD UXE-1000 (trade name; Nippon Kayaku Co., Ltd., 4-functional (meth)acrylate urethane. Hereinafter referred to as "UXE-1000") was used as (meth)acrylate urethane (C) Except for the following ratios, the same procedure as in Example 1 was carried out to prepare ink 2.
[0232] (A)HEAA 10.00g
[0233] (B)ACMO 78.00g
[0234] (C)UXE-1000 12.00g
[0235] (D)Ir754 7.00g
[0236] Using an E-type viscometer, the viscosity of the ink 2 at 25°C was measured to be 48 mPa·s.
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