Method for preparing cocoa butter equivalent by using chemical transesterification method
A technology of cocoa butter and transesterification, applied in the directions of cocoa, application, food science, etc., can solve the problems of high cost, low yield of cocoa butter-like products, and no literature reports on preparation of cocoa butter-like butter, and achieves low cost and high yield. high effect
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Embodiment 1
[0022] A method for preparing cocoa butter by chemical transesterification, comprising the following steps: taking suet oil and methyl stearate with a mass ratio of 90:10 and mixing them in a reaction Erlenmeyer flask; Dehydration and degassing under vacuum conditions of ~-0.1MPa for 30 minutes; then add high-efficiency catalyst sodium methoxide, maintain the above vacuum degree and perform esterification reaction at 90°C for 15 minutes; keep stirring, slowly add 10% of oil weight into the reaction bottle citric acid aqueous solution to terminate the reaction; then wash the reaction product with 95°C hot water for 3-4 times, and then filter to remove water to obtain the cocoa butter-like product.
[0023] A method for preparing cocoa butter by chemical transesterification, characterized in that the amount of sodium methoxide added is 0.8% of the weight of the above mixed oil.
[0024] A method for preparing cocoa butter by chemical transesterification, characterized in that th...
Embodiment 2
[0026] A kind of method that utilizes chemical transesterification method to prepare cocoa-like butter, comprises the following steps: get the suet oil, 24 degree palm oil and methyl stearate that take mass ratio and be 45:45:10 and mix and be placed in reaction Erlenmeyer flask, in 105~110℃, dehydration and degassing under vacuum conditions of -0.098~-0.1MPa for 30 minutes; then add high-efficiency catalyst sodium methoxide, maintain the above vacuum degree and perform esterification reaction at 90℃ for 15 minutes; keep stirring, pour into the reaction bottle Slowly add citric acid aqueous solution with 10% oil weight to stop the reaction; then wash the reaction product with 85°C hot water for 3-4 times, and filter to remove water to obtain the cocoa butter-like product.
[0027] A method for preparing cocoa butter by chemical transesterification, characterized in that the amount of sodium methoxide added is 0.5% of the weight of the above mixed oil.
[0028] A method for pre...
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