Method for manufacturing NdFeB permanent magnet material with co-associated mixed rare earth
A technology of mixed rare earth and permanent magnet materials, applied in the direction of magnetic materials, magnetic objects, electrical components, etc., can solve the problems of polluted environment and backlog, and achieve the effect of reducing pollution, improving microstructure, and simplifying separation steps.
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[0031] (1) The raw material is the co-associated mixed rare earths of Baiyun Obo Mine, whose composition is La: 25.87%, Ce: 53.56%, Pr: 6.59%, Nd: 13.98%, and the composition of the main alloy (by weight): MM: 33% , Fe: 64.95%, B: 1.05%, Al: 1%, auxiliary alloys are PrNd: 0.2%, NdCu: 0.2%, AlCu: 0.1%.
[0032] (2) Surface treatment of raw materials: Remove the oxides on the surface of the prepared waste and metal materials by mechanical or chemical methods.
[0033] (3) Smelting: The main alloy MMFeB is prepared into quick-setting sheets through the quick-setting process, the rotation speed is about 1-3m / s, the thickness is 0.01-2mm, and the crystallization state is controlled to be columnar.
[0034] (4) Milling: Use hydrogen explosion plus high-pressure nitrogen jet mill to grind the main alloy quick-setting sheet alloy into 3-5μm more uniform particles, and the auxiliary alloys PrNd, NdCu, AlCu, etc. through hydrogen explosion, jet mill, high-energy ball mill , Grinding in...
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