Waterborne acrylic resin and packaging container coating and preparation method

A water-based acrylic and acrylic technology, applied in the chemical industry, can solve the problems of thick coating foaming and poor fullness, and achieve the effects of improving resin weather resistance, fullness and wide application.

Inactive Publication Date: 2014-10-01
西北永新涂料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Another object of the present invention is to provide a kind of water-based packaging container coating with excellent water resistance and hig

Method used

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  • Waterborne acrylic resin and packaging container coating and preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Embodiment 1, prepare waterborne acrylic resin

[0033] The amount of raw materials is as follows: butanol (Jiangsu Sanmu) 20kg; 1,1-dimethyl-1-heptyl carboxyglycidyl ester (Shell) 10kg; acrylic acid (Beijing Dongfang) 4kg; butyl acrylate (Beijing Dongfang) 15kg; Ethylene (PetroChina) 20kg; hydroxypropyl acrylate (Nanjing) 10kg; 2-ethylhexyl acrylate (Beijing Dongfang) 12kg; tert-butyl benzoyl peroxide (Lanzhou Auxiliary Factory) 1kg; 2-amino-2 - Methyl-1-propanol (Dow Chemical) 5 kg; make up the balance with deionized water.

[0034] Formulated from 1,1-dimethyl-1-heptylcarboxyglycidyl ester, acrylic acid, butyl acrylate, styrene, hydroxypropyl acrylate, 2-ethylhexyl acrylate, tert-butyl benzoyl peroxide The mixed solution formed; put butanol into the bottom of the reactor and raise the temperature to 125°C; gradually add the mixed solution dropwise and react for 180 minutes to make it fully polymerized. Lower the temperature below 60°C for neutralization, the ...

Embodiment 2

[0035] Embodiment 2, preparation waterborne acrylic resin

[0036] The amount of raw materials is as follows: butanol (Jiangsu Sanmu) 25kg; 1,1-dimethyl-1-heptyl carboxyglycidyl ester (Shell) 7kg; acrylic acid (Beijing Dongfang) 6kg; butyl acrylate (Beijing Dongfang) 9kg; Ethylene (PetroChina) 13kg; hydroxypropyl acrylate (Nanjing) 15kg; 2-ethylhexyl acrylate (Beijing Dongfang) 20kg; tert-butyl benzoyl peroxide (Lanzhou Auxiliary Factory) 1kg; 2-amino-2 - Methyl-1-propanol (Dow Chemical) 4 kg; make up the balance with deionized water.

[0037] Formulated from 1,1-dimethyl-1-heptylcarboxyglycidyl ester, acrylic acid, butyl acrylate, styrene, hydroxypropyl acrylate, 2-ethylhexyl acrylate, tert-butyl benzoyl peroxide The mixed solution formed; put butanol into the bottom of the reactor and raise the temperature to 125°C; gradually add the mixed solution dropwise and react for 180 minutes to make it fully polymerized. Lower the temperature below 60°C for neutralization, th...

Embodiment 3

[0038] Embodiment 3, prepare waterborne acrylic resin

[0039] The amount of raw materials is as follows: butanol (Jiangsu Sanmu) 30kg; 1,1-dimethyl-1-heptyl carboxyglycidyl ester (Shell) 5kg; acrylic acid (Beijing Dongfang) 10kg; butyl acrylate (Beijing Dongfang) 8kg; Ethylene (PetroChina) 10kg; hydroxypropyl acrylate (Nanjing) 9kg; 2-ethylhexyl acrylate (Beijing Dongfang) 10kg; tert-butyl benzoyl peroxide (Lanzhou Auxiliary Factory) 1kg; 2-amino-2 - Methyl-1-propanol (Dow Chemical) 5 kg; make up the balance with deionized water.

[0040] Formulated from 1,1-dimethyl-1-heptylcarboxyglycidyl ester, acrylic acid, butyl acrylate, styrene, hydroxypropyl acrylate, 2-ethylhexyl acrylate, tert-butyl benzoyl peroxide The mixed solution formed; put butanol into the bottom of the reactor and raise the temperature to 125°C; gradually add the mixed solution dropwise and react for 180 minutes to make it fully polymerized. Lower the temperature below 60°C for neutralization, the pH...

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Abstract

The invention discloses a waterborne acrylic resin and a packaging container coating and a preparation method. The packaging container coating is prepared to solve the problem that the existing waterborne stoving varnish is blistered in thickness and poor in fullness. The preparation method of the waterborne acrylic resin comprises the following steps: adjusting the monomer proportion; modifying through 1, 1-dimethyl-1-heptyl carboxyl glycidyl ester; neutralizing through 2-amino-2-methyl-1-propanol; salifying; and realizing waterborne property to prepare the waterborne acrylic resin which is low in viscosity and good in dispersity to pigments. The preparation method of the packaging container coating comprises the following steps: selecting amino resin; quickly curing without acid catalysis; and preparing a netty crosslinking coating with excellent performance by adopting various pigments and filler. The problem that the waterborne stoving varnish is blistered in thickness is effectively improved, the water resistance of the film is enhanced, the tensile strength is improved, and the fullness of the film is improved.

Description

technical field [0001] The invention belongs to the technical field of chemical industry, and in particular relates to a water-based acrylic resin, a packaging container coating and a preparation method thereof. Background technique [0002] At present, protecting the environment has become a common issue for human beings all over the world. For paint coating, organic solvents and decomposition products produced in the drying process of various paints are discharged into the atmosphere, causing air pollution and causing great harm. In order to protect the environment, countries all over the world have successively formulated emission standards to strictly control volatile organic compounds (VOC). my country has formulated mandatory standards for the coatings industry. The government's standards on VOC emission limits have played an important role in promoting the technological development of the coatings industry. [0003] The packaging container coating industry is still ...

Claims

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Application Information

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IPC IPC(8): C08F212/08C08F220/18C08F220/06C08F220/28C09D125/14C09D133/08
Inventor 李华明张福云许玉霞李彩虹张彦芸方丽
Owner 西北永新涂料有限公司
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