Fluidized bed reactor and its application
A fluidized bed reactor and reaction tube technology, applied in chemical instruments and methods, gaseous chemical plating, carbon preparation/purification, etc., can solve the problems of poor back-mixing effect, low mass and heat transfer efficiency of the reactor, and the impact of Yield and other issues, to achieve the effect of easy processing and manufacturing, uniform gas-solid phase contact, and easy maintenance
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Embodiment 1
[0054] Carbon nanotubes are prepared by chemical vapor deposition, and the reaction equipment adopts figure 1 The fluidized bed reactor shown (the fluidized bed reactor is a variable diameter fluidized bed reactor).
[0055] The catalyst particles of growing carbon nanotubes with a certain particle size are dropped into the gas distribution plate 500 inside the fluidized bed reactor from the inlet pipe 410 of the reaction tube 100; the carrier gas is introduced into the inlet pipe 410 to adjust the carrier gas velocity, Make the catalyst particles on the gas distribution plate 500 form a well-back-mixed vortex fluid in the heating zone of the reaction tube 100; turn on the heating assembly 700, and then add the carbon-containing raw material gas required for chemical vapor deposition into the carrier gas; adjust the gas The flow rate enables continuous fluidization of the generated carbon nanotube particles. Since the density of the generated carbon nanotube particles is smal...
Embodiment 2
[0059] Porous carbon is prepared by pyrolysis, and the reaction equipment adopts figure 1 The fluidized bed reactor shown (the fluidized bed reactor is a variable diameter fluidized bed reactor).
[0060] Put the precursor particles of a certain particle size for preparing porous carbon from the inlet pipe 410 of the reaction tube 100 into the gas distribution plate 500 inside the fluidized bed reactor; feed the carrier gas into the inlet pipe 410 to adjust the carrier gas flow rate , so that the precursor particles on the gas distribution plate 500 can form a vortexized fluid with good back-mixing in the heating area of the reaction tube 100; turn on the heating component 700, and adjust to the reaction temperature of thermal cracking. Since the density of the generated porous carbon particles is lower than that of the precursor particles, the generated porous carbon particles will float to the upper part of the reaction tube 100, but since the diameter of the reaction tube...
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