Temperature-resistant salt-resistant HPAM/Cr<3+>/phenolic aldehyde compound crosslinked weak gel profile adjusting and water plugging agent and preparation method thereof
A profile control water shutoff agent, heat-resistant and salt-resistant technology, applied in the direction of chemical instruments and methods, drilling compositions, etc. Good salt performance, high gel strength, and improved heat and salt resistance
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Embodiment 1
[0046] First weigh each raw material according to the following amounts:
[0047] Partially hydrolyzed polyacrylamide (HPAM): 0.10%
[0048] Metal crosslinking agent: 0.001%
[0049]Organic crosslinking agent: 0.03%
[0050] Ammonium chloride: 0.2%
[0051] The remainder is water;
[0052] Add ammonium chloride into water and stir to make it fully dissolved; then add partially hydrolyzed polyacrylamide and stir with a stirrer for 30 minutes, then age at room temperature for 12 hours. After 12 hours, add the metal cross-linking agent and stir evenly, then place it at room temperature for 6 hours to obtain a weak gel complexed by metal ions; add the organic cross-linking agent to the synthesized weak gel, stir it evenly and place it Keep the temperature in a water bath at 75°C for 24 hours to allow polymerization to occur, and a reddish-brown viscous colloid is obtained, which is the heat-resistant and salt-resistant HPAM / Cr 3+ / Finished product of phenolic composite cross...
Embodiment 2
[0054] First weigh each raw material according to the following amounts:
[0055] Partially hydrolyzed polyacrylamide (HPAM): 0.10%
[0056] Metal crosslinking agent: 0.001%
[0057] Organic crosslinking agent: 0.04%
[0059] The remainder is water;
[0060] Ammonium oxalate was added to water and stirred to fully dissolve it; then partially hydrolyzed polyacrylamide was added and stirred with a stirrer for 30 minutes, then aged at room temperature for 12 hours. After 12 hours, add the metal cross-linking agent and stir evenly, then place it at room temperature for 6 hours to obtain a weak gel complexed by metal ions; add the organic cross-linking agent to the synthesized weak gel, stir it evenly and place it Keep the temperature in a water bath at 75°C for 24 hours to allow polymerization to occur, and a reddish-brown viscous colloid is obtained, which is the heat-resistant and salt-resistant HPAM / Cr 3+ / Finished product of phenolic compo...
Embodiment 3
[0062] First weigh each raw material according to the following amounts:
[0063] Partially hydrolyzed polyacrylamide (HPAM): 0.15%
[0064] Metal crosslinking agent: 0.002%
[0065] Organic crosslinking agent: 0.02%
[0066] Glacial acetic acid: 0.1%
[0067] The remainder is water;
[0068] Add glacial acetic acid into water, and stir; to fully dissolve it; then add partially hydrolyzed polyacrylamide, and stir with a stirrer for 30 minutes, then age at room temperature for 12 hours. After 12 hours, add the metal cross-linking agent and stir evenly, then place it at room temperature for 6 hours to obtain a weak gel complexed by metal ions; add the organic cross-linking agent to the synthesized weak gel, stir it evenly and place it Keep the temperature in a water bath at 75°C for 24 hours to allow polymerization to occur, and a reddish-brown viscous colloid is obtained, which is the heat-resistant and salt-resistant HPAM / Cr 3+ / Finished product of phenolic composite cro...
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