Soil nitrate nitrogen extracting agent and method for rapid determination of soil nitrate nitrogen
A rapid determination and nitrate nitrogen technology, applied in the field of agrochemical analysis, can solve the problems of corrosion of detection instruments and equipment, no obvious progress, environmental threats, etc., to save detection costs, reduce interference ion leaching, and have a wide range of applications.
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Embodiment 1
[0021] The rapid assay method of present embodiment soil nitrate nitrogen content comprises the following steps:
[0022] (1) Extraction: Take a fresh soil sample with a weight of 10 g through a 2 mm hole sieve, add it to a KCl aqueous solution with a volume of 50 mL and a concentration of 0.5 mol / L, oscillate for 1 to 1.5 hours, and then let it stand for 3 to 5 minutes. Filter with quantitative filter paper to obtain soil sample extract;
[0023] (2) Establish a standard curve: pipette 0.5, 1, 2, 3, 4, 5ml of 50mg / L nitrate nitrogen standard solution into a 50ml volumetric flask, then dilute to 50ml with 0.5mol / L KCl solution, Obtain gradient solutions with nitrate nitrogen concentrations of 0.5, 1, 2, 3, 4, and 5 mg / L respectively; use 0.5 mol / L KCl solution as a contrast, and use a dual-wavelength method for colorimetric determination at 220nm and 275nm wavelengths, formulate Get the corresponding standard working curve;
[0024] (3) Colorimetry: With 0.5mol / L KCl solutio...
Embodiment 2
[0027] Except that the KCl solution is 0.6 mol / L, other steps and parameters are the same as in Example 1.
Embodiment 3
[0029] Except that the KCl solution is 0.8mol / L, other steps and parameters are the same as in Example 1.
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