Preparation method of collagen modified superfine acrylic fiber
A collagen modification technology, applied in spinning solution preparation, artificial filament heat treatment, filament/thread forming, etc., can solve the problems of complex operation, poor hydrophilicity, environmental pollution, etc., and achieve soft hand feeling and good moisture absorption Sex, improve the effect of poor hydrophilicity
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Embodiment 1
[0019] Dissolve polyacrylonitrile in a solvent with a mass ratio of 1:9, add 10% polyvinylpyrrolidone, and stir evenly to prepare a fiber polymer solution; the solvent is dimethylacetamide.
[0020] In an environment of 40°C, add 3% collagen solution to the fiber polymer solution, the mass ratio of the fiber polymer solution to the collagen solution is 5:1, stir until uniform by magnetic force, and use it as a spinning solution after standing for 1 hour.
[0021] Add the spinning solution to the electrospinning machine for electrospinning, the additional electric field strength is 0.2kv / cm, the distance between the receiving screen and the spinneret is 10cm, and the calcination temperature is 400°C to obtain collagen modified ultrafine fibers .
Embodiment 2
[0023] Dissolving polyacrylonitrile in a solvent with a mass ratio of 1:5, adding 10% polyvinylpyrrolidone, and stirring evenly to prepare a fiber polymer solution; the solvent is dimethylformamide.
[0024] At 40°C, add 7% collagen solution to the fiber polymer solution, the mass ratio of the fiber polymer solution to the collagen solution is 3:1, stir until uniform by magnetic force, and use it as a spinneret solution after standing for 2 hours.
[0025] Add the spinning solution to the electrospinning machine for electrospinning, the additional electric field strength is 2kv / cm, the receiving screen is 45cm away from the spinneret, and the calcination temperature is 650°C to obtain collagen modified ultrafine fibers.
Embodiment 3
[0027] Dissolving polyacrylonitrile in a solvent with a mass ratio of 1:6, adding 10% polyvinylpyrrolidone, and stirring evenly to prepare a fiber polymer solution; the solvent is dimethylformamide.
[0028] In an environment of 40°C, add 5% collagen solution to the fiber polymer solution, the mass ratio of the fiber polymer solution to the collagen solution is 4:1, stir until uniform by magnetic force, and use it as a spinning solution after standing for 1 hour.
[0029] The spinning solution was added to the electrospinning machine for electrospinning, the additional electric field strength was 1kv / cm, the receiving screen was 25cm away from the spinneret, and the calcination temperature was 550°C to obtain collagen modified ultrafine fibers.
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