Antibacterial packaging film and preparation method thereof
A packaging film and antibacterial agent technology, applied in the field of antibacterial packaging film and its preparation, can solve the problems of low cost, antibacterial effect cannot meet market demand, etc., achieve excellent antibacterial performance, inhibit microbial growth, and easy control of process parameters.
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Embodiment 1
[0032] 1) Take an appropriate amount of β-cyclodextrin, dissolve and stir it with a certain amount of distilled water to form a β-cyclodextrin solution with a mass concentration of 10%, take an appropriate amount of camellia oil essential oil, and prepare a 10% camellia oil sesame oil with an ethanol solution After the solution was added dropwise to an equal volume of β-cyclodextrin aqueous solution. Stir at 40°C for 10 minutes and take it out. After the solution is cooled to room temperature, put it in the refrigerator and filter it with suction. The filter residue is washed with absolute ethanol and distilled water respectively, and dried at 80°C to constant weight to obtain micro Capsule product, microcapsule structure such as figure 1 shown. Sampling to test the entrapment rate of the microcapsules;
[0033] 2) Take a certain amount of chitosan and add concentration of 1% acetic acid to stir, completely dissolve, and obtain a chitosan solution with a mass concentration o...
Embodiment 2
[0037] 1) Take an appropriate amount of β-cyclodextrin, dissolve and stir it with a certain amount of distilled water to form a β-cyclodextrin solution with a mass concentration of 10%, take an appropriate amount of camellia oil essential oil, and prepare a 10% camellia oil sesame oil with an ethanol solution After the solution was added dropwise to an equal volume of β-cyclodextrin aqueous solution. Stir at 40°C for 10 minutes and take it out. After the solution is cooled to room temperature, put it in the refrigerator and filter it with suction. The filter residue is washed with absolute ethanol and distilled water respectively, and dried at 80°C to constant weight to obtain micro Capsule product. Sampling to test the entrapment rate of the microcapsules;
[0038] 2) Take a certain amount of chitosan and add concentration of 1% acetic acid to stir and dissolve completely to obtain a chitosan solution with a mass concentration of 40%; add an equal volume of tea oil with a ma...
Embodiment 3
[0042] 1) Take an appropriate amount of β-cyclodextrin, dissolve and stir it with a certain amount of distilled water to form a β-cyclodextrin solution with a mass concentration of 10%, take an appropriate amount of camellia oil essential oil, and prepare a 10% camellia oil sesame oil with an ethanol solution After the solution was added dropwise to an equal volume of β-cyclodextrin aqueous solution. Stir at 40°C for 10 minutes and take it out. After the solution is cooled to room temperature, put it in the refrigerator and filter it with suction. The filter residue is washed with absolute ethanol and distilled water respectively, and dried at 80°C to constant weight to obtain micro Capsule product. Sampling to test the entrapment rate of the microcapsules;
[0043] 2) Take a certain amount of chitosan and add concentration of 1% acetic acid to stir and dissolve completely to obtain a chitosan solution with a mass concentration of 40%; add an equal volume of tea oil with a ma...
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