Oil-in-water type water-soluble antioxidant compound and preparation method thereof

A water-soluble composite and anti-oxidant technology, which is used in food ingredients as antioxidants, food science, food preservation, etc., can solve the problems of greatly reduced anti-oxidation function, poor solubility, demulsification, etc., and achieve no loss of anti-oxidation ability, No microbial growth, the effect of increasing the surface area

Active Publication Date: 2015-01-21
HANGZHOU WAHAHA TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, natural vitamin E is an oil-soluble antioxidant and insoluble in water, and water is the most important ingredient in this type of product. Although natural VE can be added to products by means of shearing and homogenization, whether VE is good It is doubtful that the dispersion in the product system will contact with fat and exert antioxidant function
The cost of natural VE is relatively high. If the dispersion effect is not good, the anti-oxidation function will be greatly reduced, and the cost of the product will increase accordingly.
At present, there are researches to prepare water-soluble VE emulsion by dispersing VE in water by emulsification or embedding method. However, this method usually requires the use of a large amount of emulsifier, which brings poor sensory experience in the product. At the same time, VE and water A large difference in viscosity will lead to poor stability of the emulsion, which is prone to delamination or demulsification
[0004] Other food antioxidants also have many problems such as poor antioxidant effect, poor solubility, bad taste, and regulations not allowed, so they are not suitable for use in fat-containing foods with water as the carrier.
[0005] Tea polyphenols have strong antioxidant capacity, good water solubility, good stability, natural source, free radical scavenging ability and metal ion chelating ability, but they have the problem of bitter taste and poor taste, which limits their use
Compound VE with tea polyphenols, but the former is oil-soluble, while the latter is more water-soluble, and it is difficult to achieve the goal of good antioxidant capacity and stability by simple mixing

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] A preparation method of emulsified water-soluble composite antioxidant, comprising the following steps:

[0037] (1) Add 0.8kg of Span-60 to 91.1kg of glycerin preheated to 65°C, cut at 2500rpm for 10min, and obtain mixed solution A;

[0038] (2) Add 8 kg of natural vitamin E preheated to 65°C to the mixture A, cut at 2500 rpm for 15 minutes at 65°C, and pre-emulsify to obtain the mixture B;

[0039] (3) Add 0.1 kg of green tea extract to the mixed solution B, and cut at 2500 rpm for 20 minutes at 65°C to obtain the mixed solution C;

[0040] (4) Homogenize the mixed solution C at 65° C. with a high-pressure homogenizer under a pressure of 20 MPa and circulate it 4 times to obtain an emulsified water-soluble composite antioxidant.

Embodiment 2

[0042] A preparation method of emulsified water-soluble composite antioxidant, comprising the following steps:

[0043] (1) Add 2kg of Span-60 to 77.7kg of glycerin preheated to 80°C, cut at 3500rpm for 5min, and obtain mixed solution A;

[0044] (2) Add 20 kg of natural vitamin E preheated to 80°C to the mixture A, cut at 3500 rpm for 10 minutes at 80°C, and pre-emulsify to obtain the mixture B;

[0045] (3) Add 0.3 kg of green tea extract to the mixed solution B, and cut at 3500 rpm for 15 minutes at 80°C to obtain the mixed solution C;

[0046] (4) Homogenize the mixed solution C at 80° C. with a high-pressure homogenizer at a pressure of 35 MPa and circulate it twice to obtain an emulsified water-soluble composite antioxidant.

Embodiment 3

[0048] A preparation method of emulsified water-soluble composite antioxidant, comprising the following steps:

[0049] (1) Add 0.4kg of Span-60 and 0.1kg of Tween-60 to 94.45kg of glycerin preheated to 80°C, cut at 3500rpm for 5min, and obtain the mixture A;

[0050] (2) Add 5 kg of natural vitamin E preheated to 80°C to the mixture A, cut at 3500 rpm for 10 minutes at 80°C, and pre-emulsify to obtain the mixture B;

[0051](3) Add 0.05 kg of green tea extract to the mixed solution B, and cut at 3500 rpm for 15 minutes at 80°C to obtain the mixed solution C;

[0052] (4) Homogenize the mixed solution C at 80° C. with a high-pressure homogenizer at a pressure of 35 MPa and circulate it twice to obtain an emulsified water-soluble composite antioxidant.

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PUM

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Abstract

The invention discloses an oil-in-water type water-soluble antioxidant compound and a preparation method thereof. The oil-in-water type water-soluble antioxidant compound is prepared from the following components in percentage by mass by mixing: 71.5-94.45% of glycerol, 5-25% of natural vitamin E, 0.5-3% of an emulgator and 0.05-0.5% of green tea extract. The oil-in-water type water-soluble antioxidant compound is high in oxidation resistance, and is good in water solubility, stability and mouthfeel.

Description

technical field [0001] The invention relates to the field of food technology, in particular to an emulsified water-soluble composite antioxidant and a preparation method thereof. Background technique [0002] Foods with water as the main carrier, such as dairy products and vegetable protein drinks, are easily oxidized by oxygen, light, high temperature, metal ions, etc. because they are rich in unsaturated fatty acids, resulting in rancidity and destroying the product stability system. In order to avoid or delay the oxidation of fat in this type of product, in addition to avoiding various conditions that easily lead to fat oxidation during the entire production and distribution process, it is usually necessary to add antioxidants to the product. [0003] Natural vitamin E (VE) has strong antioxidant capacity, light resistance, and good thermal stability. Compared with synthetic antioxidants, it comes from nature and is more in line with modern consumers' pursuit of natural d...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L3/3544A23L3/349A23L3/3472
CPCA23L3/3472A23L3/349A23L3/3544A23V2002/00A23V2200/02A23V2250/6406A23V2250/712A23V2250/214
Inventor 马海然舒成亮薛玉清余立意李言郡欧凯
Owner HANGZHOU WAHAHA TECH
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