Flame-retardant lubricating grease composition and preparation method thereof
A technology of grease composition and flame retardant, which is applied in the field of grease, can solve problems such as excessive accumulation, fire, splashing, etc., and achieve the effects of good stability, strong anti-wear extreme pressure, and good flame retardancy
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Embodiment 1
[0027] (1) Weigh 85kg of 68# rail oil, 10kg of dienyl succinimide, 3.2kg of 4,4-dimethylazolidine and 0.5kg of sodium dodecylsulfonate, and stir evenly at 80°C.
[0028] (2) Add 3kg of zinc borate, 3kg of toluene diisocyanate, 1.8kg of graphite, 0.2kg of ammonium polyphosphate, 1.8kg of polyvinyl alcohol and 0.5kg of 2,6-di-tert-butyl p-cresol to the product of step 1, and put in In the reaction kettle, heated to 56° C. at a pressure of 1.2 MPa, reacted for 0.5 hour, homogenized and degassed, and obtained a flame-retardant grease composition.
[0029] The performance test results of the prepared flame retardant grease composition are shown in Table 1.
Embodiment 2
[0031] (1) Weigh 80kg of 5# spindle oil, 12kg of dienyl succinimide, 3.2kg of 4,4-dimethylazolidine and 3kg of sodium dodecylsulfonate, and stir evenly at 80°C.
[0032] (2) Add 4kg of zinc borate, 2kg of toluene diisocyanate, 2kg of graphite, 0.4kg of ammonium polyphosphate, 1.6kg of polyvinyl alcohol and 0.5kg of 2,6-di-tert-butyl-p-cresol to the product of step 1, and put it into reaction In the kettle, heat to 56° C. at a pressure of 0.5 MPa, react for 0.5 hour, homogenize and degas to obtain a flame retardant grease composition.
[0033] The performance test results of the prepared flame retardant grease composition are shown in Table 1.
Embodiment 3
[0035] (1) Weigh 75 kg of polyalphaolefin, 14 kg of dienyl succinimide, 3.6 kg of 4,4-dimethylazolidine and 1.5 kg of sodium dodecylsulfonate, and stir evenly at 80°C.
[0036] (2) Add 5kg of zinc borate, 3kg of toluene diisocyanate, 1.8kg of graphite, 0.4kg of ammonium polyphosphate, 1.6kg of polyvinyl alcohol and 1kg of 2,6-di-tert-butyl-p-cresol to the product of step 1, and put it into reaction In the kettle, heat to 60° C. at a pressure of 1.2 MPa, react for 1 hour, and homogenize and degas to obtain a flame-retardant grease composition.
[0037] The performance test results of the prepared flame retardant grease composition are shown in Table 1.
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