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Method for connecting carbon nanometer tube macroscopic material with metal

A carbon nanotube and metal connection technology, applied in the field of nanomaterials, can solve problems such as excessive contact resistance, large contact resistance, and few researches, and achieve the effects of reduced connection resistance, short curing time, and simple equipment

Active Publication Date: 2015-02-25
北京旭江科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These two methods will cause excessive contact resistance, and some even reach the gigaohm level. Even if the second method is followed up, such as electron beam bombardment, high temperature annealing, etc., there will still be too large contact resistance, reaching Dozens or even hundreds of ohms
Moreover, the above work is limited to the contact between microscopic carbon nanotubes and metal electrodes, and there is little research on the contact between macroscopic carbon nanotubes and macroscopic metals.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Use No. 01 sandpaper to polish and polish the 0.2 mm-diameter linear metal copper part to be connected. When the surface metal at this position is polished and has a metallic luster, clean and polish the part with ethanol, so that the surface of the connection part is clean and rough. The surface is easy to absorb the coating material, and then it is placed in the air to dry naturally for 10 minutes, so that the ethanol for cleaning can be fully removed. Prepare a carbon nanotube macroscopic film with an area of ​​5*5 mm, prepare 0.1 mL of room temperature curing silver glue, measure its resistivity before use, and keep its resistivity within the range of 0.002-0.01 Ω / cm to ensure After the resistivity of the silver glue meets the conditions, apply the silver glue to the carbon nanotube macroscopic film to be connected through the needle tip of a 1 mL syringe, and spread it flat with a soft brush, so that the silver glue can be spread evenly on the coated carbon nanotube...

Embodiment 2

[0020] The parts to be connected of linear aluminum with a diameter of 0.5 mm are polished and polished with No. 01 sandpaper. When the surface metal at this position is polished and has a metallic luster, clean and polish the parts with ethanol, so as to clean the surface of the connected parts and maintain a rough surface. It is easy to absorb the coating material, and then place it in the air to dry naturally for 20 minutes, so that the ethanol for cleaning can be fully removed. For carbon nanotube macroscopic fibers with a diameter of 1 mm and a length of 100 mm, prepare 0.2 mL of room temperature curing silver glue, measure its resistivity before use, and keep the resistivity within the range of 0.002-0.01 Ω / cm to ensure that the silver After the resistivity of the glue meets the conditions, apply the silver glue to the macroscopic fiber part of the carbon nanotubes to be connected through the needle tip of a 1 mL syringe, and spread it flat with a soft brush, so that the ...

Embodiment 3

[0022]Use No. 01 sandpaper to polish and polish the 1.5 mm diameter linear metal tin to be connected. When the surface metal at this position is polished and has a metallic luster, clean and polish the polished part with ethanol, so that the surface of the connected part is clean and rough. The surface is easy to absorb the coating material, and then it is placed in the air to dry naturally for 30 minutes, so that the ethanol for cleaning can be fully removed. Prepare a macroscopic film of carbon nanotubes with an area of ​​40*40 mm, and prepare 0.3 mL of silver glue cured at room temperature. Measure its resistivity before use, and keep the resistivity within the range of 0.002-0.01 Ω / cm to ensure the resistance of the silver glue After the rate meets the conditions, apply the silver glue to the carbon nanotube macroscopic film to be connected through the needle tip of a 1 mL syringe, and spread it flat with a soft brush, so that the silver glue can be spread evenly on the coa...

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Abstract

The invention provides relates to connection technologies for carbon nanometer tube macroscopic films or fibers and metal in the technical field of nanometer materials, in particular to a method for connecting a carbon nanometer tube macroscopic material with metal. The method sequentially comprises the following steps that the portion, needing to be connected, of line-shaped or band-shaped metallic copper or metallic aluminum or metallic tin is ground, polished, washed with ethyl alcohol and dried; carbon nanometer tube macroscopic films or fibers are well prepared, 0.01 mL to 10 mL of elargol is cured at a room temperature, after it is guaranteed that the condition that the curing electric resistivity is kept between 0.002 Ohm / cm to 0.01 Ohm / cm is met, the portion, needing to be connected, of the carbon nanometer tube macroscopic material is coated with the elargol through a needle point of an injector, the metallic portion needing to be connected with the carbon nanometer tube macroscopic material is placed on the surface coated with the elargol, the metal is tightly pressed through a steel ruler, and then the metal can be completely connected with the carbon nanometer tube macroscopic films or fibers. By the adoption of the method for connecting the carbon nanometer tube macroscopic material with the metal, the obtained contact resistance between carbon nanometer tube macroscopic material and the metal is reduced to within 10 Ohms, the technology is simple, and cost is low.

Description

technical field [0001] The invention relates to a connection technology of carbon nanotube macroscopic film or fiber and metal in the technical field of nanometer materials, which can reduce the contact resistance between the two. Background technique [0002] As a new type of nanomaterial, carbon nanotubes have great potential application advantages due to their excellent electrical properties, thermal properties, and electromagnetic properties since they were discovered. Especially for those applications in the research fields of nanoelectronics, nanochemistry, and nanomaterials, it has broad application prospects. When carbon nanotubes are used as conductive or thermally conductive materials, it is inevitable to contact with other materials to form a loop. Therefore, the contact between carbon nanotubes and other materials plays a very important role. However, due to the small diameter of carbon nanotubes, the macroscopic carbon nanotube fibers or films are also composed...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01R4/62B81C99/00
CPCB81C99/00H01R4/62
Inventor 吴子平尹艳红胡英燕赵曼羊建高
Owner 北京旭江科技有限公司
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