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A kind of preparation method of modified medical stone

A medical stone and modification technology, applied in chemical instruments and methods, silicates, inorganic chemistry, etc., can solve the problems of limited ammonia nitrogen adsorption and removal capacity, achieve good practical application value and industrialization prospects, simple operation, The effect of the augment function

Inactive Publication Date: 2016-10-19
符瞰
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the existing natural medical stone has limited adsorption and removal capacity for ammonia nitrogen and heavy metals, so it is necessary to improve the medical stone to improve its adsorption capacity for ammonia nitrogen.

Method used

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  • A kind of preparation method of modified medical stone

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Embodiment Construction

[0022] A kind of preparation method of modified medical stone created by the present invention is used to prepare medical stone with high adsorption and removal ability to ammonia nitrogen and heavy metals. First, the medical stone is placed in an electric blast drying oven at 100 Roast at ~ 110 ℃ for 1 hour, then let it cool to room temperature, crush it, and sieve it with 40 mesh and 80 mesh sieve to obtain medical stone with particle size between 80 and 40 mesh.

[0023] Then soak the medical stone in 5 steps.

[0024] First, prepare a 1mol / L hydrogen chloride solution, mix medical stone and hydrogen chloride solution at a ratio of 1:10, soak in ultrasonic waves with a power of 60W and a frequency of 10000Hz for 1 hour at room temperature, and then use an 80-mesh sieve to crush The powder residue was washed twice with ionized water, then dried at 120°C for 1 hour, and at 100°C for 1 hour.

[0025] Second, prepare a 0.2mol / L sodium chloride solution, mix the medical stone o...

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Abstract

The invention creatively discloses a preparation method of modified medical stone. The preparation method of the modified medical stone comprises the following steps: roasting the medical stone, then crushing the medical stone, screening to extract the medical stone with a particle size of 40-80 meshes, soaking the medical stone with a hydrogen chloride solution by radiation of ultrasonic wave with power of 60W, dipping the medical stone with a sodium chloride solution under negative pressure of 10-30 MPa, soaking the medical stone with a lithium chloride solution at 25 DEG C by oscillating at a rate of 180 r / min, soaking the medical stone with an aluminum chloride solution at 90 DEG C by oscillating at a rate of 100 r / min and soaking the medical stone with hydrogen peroxide step by step. According to the soaked medical stone, the ion exchange capability and the adsorption capability of the medical stone are greatly improved; the medical stone can be used for adsorbing and removing ammonia nitrogen and heavy metal ions; the effect of purifying water is achieved.

Description

technical field [0001] The invention relates to the technical field of medical stone, in particular to a preparation method of modified medical stone. Background technique [0002] With the destruction of water environment caused by population and economic growth, the shortage of water resources is increasing day by day. Water treatment has attracted people's attention. Traditional techniques like coagulation, sedimentation, filtration, and adsorption have been widely used to remove pollutants in water. Among them, adsorption technology has always been the focus of research and development because of its low cost, high efficiency, and easy promotion. However, the high cost and low efficiency of adsorbents limit the application of this technology. The development of new, high-efficiency, low-cost and abundant sources of new mineral adsorbents has always been a hot spot. [0003] Medical stone is a compound mineral or medicinal rock that is non-toxic and harmless to living t...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J20/16B01J20/30C02F1/28
CPCB01J20/165B01J20/3204B01J20/3214C02F1/281
Inventor 符瞰钟同畅
Owner 符瞰
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