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Preparation process of lithium battery slurry

A preparation process, lithium battery technology, applied in the direction of battery electrodes, circuits, electrical components, etc., can solve the problems of poor stability, long process time, poor quality, etc., and achieve the effect of short process time and uniform slurry

Active Publication Date: 2015-03-25
HEBEI YINLONG NEW ENERGY +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, most of the current processes still use the traditional slurry preparation process, and the high-speed dispersion process is used to disperse the slurry. The slurry prepared by this process is prone to agglomeration, poor uniformity, poor stability, and long processing time.
The performance consistency of lithium-ion batteries prepared by using this slurry is poor, which affects the assembly and use of lithium-ion batteries

Method used

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  • Preparation process of lithium battery slurry

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] In this embodiment, the positive electrode active material is lithium nickel cobalt manganese oxide, the rubber powder is PVDF (polyvinylidene fluoride), the solvent is NMP (N-methylpyrrolidone), and the conductive agent is carbon black.

[0035] Clean the mixing tank of the double planetary power mixer, add all the rubber powder and solvent accounting for 10% of the total solvent weight, turn on the revolution and stir at a low speed, control the stirring speed at 10RPM, and vacuum, the vacuum degree is -0.085MPa~-0.095MPa. When finally forming a transparent gel-like liquid, it is made into a glue solution.

[0036] At the same time, pre-mix the conductive agent with a solvent accounting for 15% of the total solvent weight, turn on the revolution and stir at a low speed, control the stirring speed at 8RPM, vacuumize, the vacuum degree is -0.085MPa~-0.095MPa, and mix well to make a conductive agent solution Pre-mix the active substance with a solvent accounting for 35% ...

Embodiment 2

[0039] In this embodiment, the positive electrode active material is lithium nickel cobalt manganese oxide, the rubber powder is PVDF (polyvinylidene fluoride), the solvent is NMP (N-methylpyrrolidone), and the conductive agent is carbon black.

[0040] Clean the mixing tank of the double planetary power mixer, add all the rubber powder and the solvent accounting for 10% of the total solvent weight, turn on the revolution and stir at a low speed, the stirring speed is controlled at 10RPM, when the rubber powder is completely soaked and appears viscous, further Add solvent accounting for 40% of the total solvent weight, revolution and stir, the stirring speed is controlled at 10RPM, vacuumize, the vacuum degree is -0.085MPa~-0.095MPa. When finally forming a transparent gel-like liquid, it is made into a glue solution.

[0041] At the same time, pre-mix the conductive agent with a solvent accounting for 15% of the total solvent weight, turn on the revolution and stir at a low sp...

Embodiment 3

[0044] In this embodiment, the negative electrode active material is lithium titanate, the rubber powder is PVDF, the solvent is NMP, and the conductive agent is carbon black.

[0045] Clean the mixing tank of the double planetary power mixer, add all the rubber powder and the solvent accounting for 15% of the total solvent weight, turn on the revolution and stir at a low speed, the stirring speed is controlled at 8RPM, when the rubber powder is completely soaked and viscous, further Add solvent accounting for 35% of the total solvent weight, revolution and stir, the stirring speed is controlled at 10RPM, and vacuumize, the vacuum degree is -0.085MPa~-0.095MPa. When finally forming a transparent gel-like liquid, it is made into a glue solution.

[0046] At the same time, pre-mix the conductive agent with a solvent accounting for 10% of the total solvent weight, turn on the revolution and stir at a low speed, control the stirring speed at 8RPM, vacuumize, the vacuum degree is -...

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Abstract

The invention discloses a preparation process of lithium battery slurry. The preparation process comprises the steps: (1) adding gelatin powder into a first stirring container, adding a first part of solvent, carrying out vacuum stirring, and uniformly mixing to obtain liquid cement, wherein the first part of solvent is 10 to 15 percent of the weight of the entire solvent; (2) adding conductive agent powder into a second stirring container, adding a second part of solvent, carrying out vacuum stirring, and uniformly mixing to obtain a conductive agent solution, wherein the second part of solvent is 5 to 15 percent of the weight of the entire solvent; (3) adding active substance powder into a third stirring container, adding a third part of solvent, carrying out vacuum stirring, and uniformly mixing to obtain an active substance solution, wherein the third part of solvent is 10 to 35 percent of the weight of the entire solvent; and (4) adding the conductive agent solution and the active substance solution into the liquid cement, adding the remaining solvent, carrying out vacuum stirring, and uniformly mixing to obtain lithium battery slurry. According to the preparation process of the lithium battery slurry, the preparation time of the slurry is short, and the prepared slurry is more uniform and good in stability.

Description

technical field [0001] The invention relates to the field of batteries, in particular to a preparation process of lithium battery slurry. Background technique [0002] Since the successful development of lithium-ion batteries, due to their unique advantages such as high specific energy, high working voltage, wide application temperature range, low self-discharge rate, long cycle life, no pollution, and good safety, they have been widely used in computers. , cameras, aerospace, artificial satellites, small medical instruments and military communication equipment and other fields. [0003] In recent decades, with the development of science and technology, lithium-ion and other related battery technologies have made great progress. But there are still some problems. The pulping process is the most important link in the entire production process of lithium-ion batteries, which has an impact on product quality of more than 30%. However, most of the current processes still use ...

Claims

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Application Information

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IPC IPC(8): H01M4/139
CPCH01M4/139Y02E60/10
Inventor 刘金良高峰张汝彬石琳琳张要枫陈蓓
Owner HEBEI YINLONG NEW ENERGY
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