Preparation method of degradable environment-friendly packaging film
A packaging film and environment-friendly technology, applied in the field of preparation of degradable and environment-friendly packaging films, can solve the problems of low production rate, high cost, complicated process, etc., and achieve high production rate, low cost and simple and reasonable process. Effect
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Embodiment 1
[0019] A preparation method of a degradable environment-friendly packaging film, comprising the following steps:
[0020] (1) Dissolving chitosan: dissolving chitosan in acetic acid solution to obtain a chitosan solution with a mass concentration of 30g / L;
[0021] (2) Preparation of hydroxypropyl methylcellulose solution: use distilled water to prepare a hydroxypropyl methylcellulose solution with a mass concentration of 10 g / L;
[0022] (3) Mixing: mix the chitosan solution prepared in step (1) with the hydroxypropyl methylcellulose solution prepared in step (2) according to the volume ratio of 1:0.8;
[0023] (4) Add metal ion compound: add the metal ion compound to the mixed solution prepared in step (3), then stir with a magnetic stirrer, degas it ultrasonically, and cast the film at 25°C;
[0024] (5) Membrane production: Put the membrane in step (4) into a drying oven to dry for 4 hours, then soak it in 2.0mol / L NaOH solution for 1 hour, take it out and wash it with wa...
Embodiment 2
[0026] All the other are identical with embodiment 1, and difference is that in described step (1), get chitosan and be dissolved in acetic acid solution, obtain the chitosan solution that mass concentration is 35g / L; Use distilled water in described step (2) The mass concentration of the configuration is 15 g / L hydroxypropyl methylcellulose solution; in the step (4), the metal ion-containing compound is added to the mixed solution prepared in the step (3), then stirred with a magnetic stirrer, and ultrasonically Degassing, then casting at 45°C to form a film;
Embodiment 3
[0028] All the other are identical with embodiment 1, and difference is that in described step (1), get chitosan and be dissolved in acetic acid solution, obtain the chitosan solution that mass concentration is 33g / L; Use distilled water in described step (2) The mass concentration of the configuration is 12g / L hydroxypropyl methylcellulose solution; in the step (4), the metal ion-containing compound is added to the mixed solution prepared in the step (3), then stirred with a magnetic stirrer, ultrasonically Gas, and then cast at 32 ° C to form a film;
[0029] Based on the above: by dissolving chitosan--preparing hydroxypropyl methylcellulose solution--mixing--adding metal ion compounds--film making five major process steps, chitosan mixed with hydroxypropyl methylcellulose simultaneously contains The metal ions can be used to prepare an environment-friendly packaging film, which also has an antibacterial effect. The technical solution of the invention has a simple and reason...
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