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Method for determining boiling loss in minced meat gelation process through low-field nuclear magnetic resonance

A low-field nuclear magnetic resonance, minced meat technology, applied in the direction of analysis using nuclear magnetic resonance, etc., can solve the problem of not being able to truly and effectively reveal the water retention properties of meat and meat products, unable to reflect the spatial distribution information of the water content of meat and meat products, destroying meat and meat products. Problems such as the structure and properties of meat products, to achieve the effect of solving high cooking loss rate, optimizing cooking temperature and time, and high yield

Active Publication Date: 2016-01-27
NANJING AGRICULTURAL UNIVERSITY
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  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the common disadvantages of these methods are that they cannot reflect the spatial distribution information of the moisture in meat and meat products, and they are destructive to the samples. The original structure and properties of meat and meat products will be destroyed during the detection, so that it cannot be real. Effectively reveal the water retention properties of meat and meat products

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  • Method for determining boiling loss in minced meat gelation process through low-field nuclear magnetic resonance
  • Method for determining boiling loss in minced meat gelation process through low-field nuclear magnetic resonance
  • Method for determining boiling loss in minced meat gelation process through low-field nuclear magnetic resonance

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Embodiment Construction

[0031] The present invention will be further described below in conjunction with accompanying drawing and specific embodiment:

[0032] Take minced meat products with a fat content of 20% as an example:

[0033] The traditional method for measuring cooking loss (moisture loss and fat loss): take about 30g of emulsified minced meat and place it in a centrifuge tube with a diameter of 50mm, and centrifuge at 560g on a high-speed centrifuge for 10min at 4°C. The fat layer and the water layer will be clearly separated, and then the water loss rate and fat loss rate in the emulsified minced meat are calculated respectively with the following formula:

[0034] Water loss (%) = mass of water layer (m l ) / total weight of emulsified meat (g)×100

[0035] Fat loss (%) = mass of fat layer (m 2 ) / total weight of emulsified meat (g)×100

[0036] LF-NMR determination of cooking loss:

[0037] (1) Raw material sample preparation: surface tendons, fascia and fat were removed from pork hi...

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Abstract

The invention discloses a method for determining the boiling loss in a minced meat gelation process through low-field nuclear magnetic resonance. The method adopting emulsified minced meat as a research object comprises the following steps: preparing a raw material, determining a sample through low-field nuclear magnetic resonance, carrying out deuteration and freeze drying on the minced meat (twice), determining through low-field nuclear magnetic resonance, and carrying out inversion and analysis on data obtained through the low-field nuclear magnetic resonance to measure and evaluate the water and fat change conditions of the minced meat with different contents of fat in the boiling process for making the emulsified minced meat form gel from sol. The method has the advantages of simple process flow, convenient operation, and suitableness for industrial production; a low-field nuclear magnetic resonance technology is adopted to carry out online real-time monitoring, so the boiling loss change in the product production process can be accurately and effectively judged; and the product boiling loss directly influences the finial yield of the product, and the boiling temperature and the boiling time can be optimized according to the boiling loss change rule provided by the low-field nuclear magnetic resonance technology to guarantee high yield of the product.

Description

technical field [0001] The invention belongs to the technical field of on-line quality monitoring of intensively processed meat products, and relates to a method for measuring the cooking loss during gelatinization of minced meat based on hydrogen proton low-field nuclear magnetic resonance technology. Background technique [0002] Low-temperature emulsified sausage is minced meat or minced meat-like products. As one of the most important products in low-temperature meat products, because of its fresh and tender taste, light and refreshing taste, rich protein content, low-temperature processing can maximize the retention of nutrients in the meat, It has increasingly become one of the favorite meat products of consumers. [0003] From the perspective of processing, low-temperature emulsified sausage is a typical heat-induced gel product. When the protein solution with a concentration exceeding a certain level is heated, the protein molecules will be resolved, folded and aggre...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N24/08
Inventor 周光宏杨慧娟薛思雯徐幸莲
Owner NANJING AGRICULTURAL UNIVERSITY
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