A kind of blended material with high acetate fiber content and preparation method thereof
A technology of cellulose acetate and cellulose acetate, which is applied in the direction of spinning solution preparation, artificial filament made of cellulose derivatives, fiber treatment, etc., can solve the problems of low dissolution rate of cellulose acetate and satisfactory strength, and achieve Good touch, wide adaptability and good air permeability
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Embodiment 1
[0024] Take ramie fiber powder and cellulose acetate powder, the crushing particle size of the above powder is less than 300 mesh;
[0025] Put the above powder into 1-butyl-3-methylimidazole chloride ionic liquid ([BMIM)Cl), including ramie fiber powder, cellulose acetate powder and 1-butyl-3-methylimidazole chloride ionic liquid The mass parts of the three are: 2.5 parts of ramie fiber powder, 11 parts of cellulose acetate powder, 100 parts of 1-butyl-3-methylimidazole chloride ionic liquid; after fully stirring, under 40 degrees Celsius and ultrasonic vibration conditions Leave it for 20-30 hours to obtain the spinning solution; after filtering and defoaming the spinning solution, perform electrostatic spinning under the action of 15-20KV voltage; then, conduct a water bath at 10-15 degrees Celsius, bleach and After drying, acetate fiber blended with ramie fiber is formed. Through the above treatment, a cellulose acetate monomer plasticized with imidazole ionic liquid is form...
Embodiment 2
[0031] Take nylon powder and cellulose acetate powder, the crushing particle size of the above powder is less than 300 mesh;
[0032] Put the above powder into chlorinated-allyl-methylimidazole hydrochloric acid ionic liquid ([AMIM)Cl), including nylon powder, cellulose acetate powder and chlorinated-allyl-methylimidazole hydrochloric acid ionic liquid. The parts are: 2.5 parts of nylon powder, 10 parts of cellulose acetate powder, 90 parts of 1-butyl-3-methylimidazole chloride ionic liquid; after fully stirring, place 20-30 under the condition of 40 degrees Celsius and ultrasonic vibration After the spinning solution is filtered and defoamed, the spinning solution is subjected to electrostatic spinning under the action of 15-20KV voltage; then, the water bath is carried out at 40-55 degrees Celsius, and then, bleached to 40- Rinse with 50% ethanol and dry to form acetate fiber blended with nylon. Through the above treatment, a cellulose acetate monomer plasticized with imidazol...
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