Preparation method of non-bending ultrafine tungsten wire for z-pinch quasi-spherical wire array

A tungsten wire and bending technology, applied in the field of preparation of non-bending ultra-fine tungsten wire, can solve problems such as difficulty in meeting the forming requirements of Z-pinch quasi-spherical wire array, not paying attention to the bending phenomenon of tungsten wire, and reducing strength.

Inactive Publication Date: 2017-05-17
LASER FUSION RES CENT CHINA ACAD OF ENG PHYSICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] Although the drawing method combined with electrochemical corrosion is widely used in the industry to prepare ultra-fine tungsten wires, the bending phenomenon of tungsten wires is not paid attention to, and the breaking strength of Φ6μm tungsten wires produced by industrial methods is lower than 2800MPa
This strength is slightly higher than the strength that the tungsten wire needs to withstand when forming a quasi-spherical wire array. However, if the tungsten wire produced by the traditional process is annealed, its strength will be further reduced, which makes it difficult to meet the forming requirements of the Z-pinch quasi-spherical wire array.

Method used

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  • Preparation method of non-bending ultrafine tungsten wire for z-pinch quasi-spherical wire array
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  • Preparation method of non-bending ultrafine tungsten wire for z-pinch quasi-spherical wire array

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preparation example Construction

[0022] According to the preparation method of the non-bending ultra-fine tungsten wire used for the Z-pinch quasi-spherical wire array of the present invention, the diameter of the ultra-fine tungsten wire is between 4 μm and 10 μm and there is no bending phenomenon within the range of centimeters. Doped tungsten wire is used as the raw material for electrolytic corrosion, and the main added elements are Mo (20 ppm) and K (85 ppm). The preparation and heat treatment of ultra-fine tungsten wire are usually divided into three steps: hot drawing, electrolytic corrosion and annealing heat treatment.

[0023] First, the raw material wire is hot-drawn to control the diameter of the raw material wire at a suitable diameter (a range greater than or equal to 16 μm), so that the first pass of electrolytic corrosion has a large bending span.

[0024] Multi-pass electrolytic corrosion process is carried out, and the ultimate single-pass diameter reduction method is used to maintain the me...

Embodiment 1

[0028] The electrolytic corrosion raw material wires of different diameters are obtained by the hot drawing method, and a slight electrolytic corrosion is carried out for one pass. The tungsten wire with a lower horizontal length of about 5 cm is counted under a microscope to check whether there is a sharp bend and the average bend span after electrolytic corrosion. Table 1 lists the measurement results. The raw material wires with a diameter of less than 16 μm have sharp bends after slight corrosion; while the raw material wires with a diameter greater than 18 μm have a longer average bending span after electrochemical corrosion, which means a larger curl radius; further increase The diameter of the raw material wire after electrochemical corrosion has little difference in the average bending span, but this will increase the number of electrochemical corrosion passes of the tungsten wire. Therefore, the present invention preferably selects a tungsten wire with a diameter of ab...

Embodiment 2

[0032]The tungsten wire with a diameter of about 21 μm is used for electrolytic corrosion, and the electrolytic voltage of 2.0V is used, and the wire receiving speed is 62.8mm / s. The diameter of the reel is 30mm, but the diameter of the reel is different. The tungsten wires were corroded to Φ6μm with different sizes of wire reels, and the tungsten wires with a horizontal length of about 5cm in the natural state were counted under a microscope, and the average bending span results were listed in Table 2. It can be seen that the average bending span of the tungsten wire is not much different from the average bending span when the diameter of the wire-receiving wheel is smaller than the diameter of the wire-releasing wheel, both are about 2.3mm; when the diameter of the wire-receiving wheel is larger than the diameter of the wire-releasing wheel, The value of the average bending span is related to the diameter of the take-up wheel; when the diameter of the take-up wheel exceeds 40...

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Abstract

The invention discloses a preparing method for non-bending ultrathin tungsten wires for a Z-pinch torispherical wire array. The diameter of the ultrathin tungsten wires ranges from four micrometers to ten micrometers, and no bending phenomenon exists in the centimeter magnitude range. The method comprises the following steps that raw material wires are subjected to hot drawing to enable the diameter to be controlled within the range larger than or equal to 16 micrometers; a multi-pass electrolytic etching technology is carried out, a limit single-pass diameter reducing method is adopted to enable the ultrathin tungsten wires obtained after continuous electrochemical corrosion to keep the mechanical property under the condition that the bending span is slightly increased; and in annealing heat treatment, the finished tungsten wires are rewound on a quartz glass tube to be placed in a heat treatment furnace so as to be heated to 480 DEG C and conduct heat preservation for 10 minutes, the tungsten wires are cooled along with cooling of the furnace, in the period, the quartz glass tube is vacuumized, high-purity argon or high-purity nitrogen is injected in to serve as protection gas, and the finished tungsten wires are recrystallized, but the breaking strength is not obviously reduced. Compared with the traditional technology, the ultrathin tungsten wires manufactured with the preparing method have the beneficial effects that no obvious bending exists in the free state, and the breaking strength is better.

Description

technical field [0001] The invention belongs to the fields of ultra-fine tungsten wire processing technology and Z-pinch target material preparation, and in particular relates to a preparation method of non-bending ultra-fine tungsten wire used for Z-pinch quasi-spherical wire arrays. Background technique [0002] The physical conception of inertial confinement fusion (ICF) driven by strong X-ray radiation generated by fast plasma pinch (Z-pinch) to drive DT fuel capsule implosion is considered to be a simple, efficient and technically feasible new way of fusion energy. In Z-pinch experimental research, in order to obtain high X-ray yield, the initial radius and wire quality of the wire array load must be optimized. Ultra-fine tungsten wire (usually 3 μm ~ 10 μm in diameter) is the most commonly used wire array target material, and the diameter parameters, straightness and mechanical performance parameters of tungsten wire are important technical indicators for tungsten wire...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B21C37/04
CPCB21C37/047
Inventor 刘旭东杨毅周秀文杨波白黎牛高余斌朱晔
Owner LASER FUSION RES CENT CHINA ACAD OF ENG PHYSICS
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