Preparation method of honeysuckle extract and application of honeysuckle extract to preservative-free cosmetics
A technology of honeysuckle extract and cosmetics, which is applied in the extraction of honeysuckle extract and antiseptic and antibacterial ingredients, which can solve the problems of excessive preservative addition, product irritation, improper selection, etc., and achieve mild and non-irritating products and skin compatibility Good, reduce irritation and allergy rate effect
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preparation example Construction
[0021] The honeysuckle extract is prepared by a preparation method comprising the following steps: after grinding the honeysuckle, taking an appropriate amount into a soaking tank and adding a certain proportion of propylene glycol aqueous solution, the solid-liquid ratio of the honeysuckle and the propylene glycol aqueous solution is 1:5-1: 60. The mass ratio of water to propylene glycol in the propylene glycol aqueous solution is 2-1:1-4, stir and soak for 8-24 hours, then transfer the treatment liquid into the extraction tank for microwave extraction, the extraction time is 5-40 minutes, and the extraction temperature is 25-125°C, microwave power 300-1500W, filter the extract to obtain honeysuckle extract.
[0022] The preferred preparation condition is that the solid-liquid ratio of honeysuckle and propylene glycol aqueous solution is 1:20, the mass ratio of water and propylene glycol in the propylene glycol aqueous solution is 1:4, stir and soak for 12 hours, then transfer...
Embodiment
[0024] 1. Selection of preparation conditions
[0025] Table 1. The content of honeysuckle extract (chlorogenic acid) obtained under different preparation conditions
[0026]
[0027] It can be seen from Table 1 that the honeysuckle extract (chlorogenic acid) prepared according to different preparation conditions of the present invention can obtain higher chlorogenic acid content, and wherein the honeysuckle extract (chlorogenic acid) prepared under the preparation conditions shown in Example 15 acid) with the highest content of 0.92 mg / g, which is the preferred preparation condition of the present invention. However, the content of the honeysuckle extract (chlorogenic acid) obtained without adopting the preparation conditions of the present invention is low.
[0028] 2. Qualitative analysis by HPLC
[0029] The spectrum below shows that the detected substance has the maximum absorption peak at 3.827min and 3.832min. It can be concluded that the two substances are the s...
specific Embodiment 1
[0053] Table 3 Adding the extract to the cosmetic cream base
[0054]
[0055] Table 4 The results of the anti-corrosion challenge experiment of Example 1 and Comparative Example 1
[0056]
[0057] The experimental results in Table 4 show that the honeysuckle extract shows good antibacterial ability in the cosmetic cream base, and can be added to cosmetics as a pure natural antiseptic and antibacterial ingredient.
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