Nanosilicon dioxide structure-based high-heavy metal ion adsorption chelating agent and preparation method thereof
A technology of heavy metal ions and chelating agents, applied in chemical instruments and methods, adsorption water/sewage treatment, other chemical processes, etc., can solve the problems of weak heavy metal ions, small specific surface area of copolymers, and few adsorption sites, etc. Fast and effective adsorption and chelation, the effect of broad application prospects
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[0007] The technical scheme of the present invention is as follows:
[0008] A high-adsorption nano-type heavy metal ion chelating agent having a structure shown in formula (I):
[0009]
[0010] In formula (I), 100≤n≤300.
[0011] According to the present invention, preferably, the specific surface area of the heavy metal ion chelating agent is 130-170m 2 / g, the grafting rate is 55-94%.
[0012] The preparation method of the above-mentioned high adsorption nano-type heavy metal ion chelating agent includes the following steps:
[0013] (1) Nano SiO 2 Surface amino modification
[0014] Nano SiO 2 Disperse uniformly in absolute ethanol by ultrasonic, add 3-aminopropyltriethoxysilane coupling agent (KH550), stir at room temperature, heat up to 70-90℃, 2 Reflux in the atmosphere, centrifugation, and the solids obtained by centrifugation are dispersed and washed in absolute ethanol, and then dried in vacuum to obtain nano-SiO 2 -NH 2 ;
[0015] (2) Nano SiO 2 -NH 2 Brominated modification...
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