35results about How to "The implementation conditions are simple" patented technology

The invention relates to a synthetic method of chabasite, which comprises the step of: adopting traditional hydrothermal synthesis to prepare chabasite through a seed crystal guiding way under a condition of not adding an organic template agent. The method avoids using expensive template agents and also avoids environmental pollution caused by high temperature firing of the template agent in a product post-treatment process. The synthetic method of the chabasite disclosed by the invention has an important significance in terms of basic research; meanwhile, as the synthetic method is economic and environment-friendly, the synthetic method also has wide application foreground.

The invention relates to a preparation method for 9, 10-dihydroxy stearic acid and methyl ester, which is characterized in that the oleic acid and the formic acid are mixed uniformly in room temperature; the mixture is added with hydrogen peroxide, and warmed up and separated from water phase; the solvent is recycled through decompression and distillation; the generative reaction admixture is recrystallized with organic solvent, so that the product 9, 10-dihydroxy stearic acid is prepared. The recovered formic acid solution can generate ice-cream calcium formate salt separation by adding calcium oxide and calcium carbonate; subsequently the methyl alcohol and oil of vitriol is arranged into the product 9, 10-dihydroxy stearic acid for a reflux reaction, and then is rotated and vaporized out the water phase and oil phase for being washed to be neutral, thereby the 9, 10-dihydroxy stearic acid methyl ester product is generated through dehydration. The invention has the advantages of clean process, safe implementation, easy operation, full utilization of the reactant, reduced waste emission, effective utilization of the low-concentration hydrogen peroxide, and favorableness to large-scale production.

The invention mainly introduces a method for fast synthesizing high-crystallinity and high-yield fluoride-free AlPO4-34 through a mixed solvent hot process under the condition without hydrofluoric acid by using common organic amine morpholine as template agents and mixing isopropanol or ethylene glycol and water according to certain proportions. In the method, firstly, aluminum sources, phosphor sources, water, sopropanol or ethylene glycol and organic template agents are uniformly mixed in a certain sequence according to a certain mol rate that Al2O3/P2O5/morpholine/H2O/R (isopropanol or ethylene glycol)=1.0/0.8 to 1.2/2.0 to 8.0/12.5 to 75/4.0 to 24, the stirring and the ageing are carried out, the mixture is transferred into a stainless steel reaction kettle for being crystallized for 1 to 6 days at 170 to 200 DEG C at self generated pressure, then, sudden cooling, collection, filtering, washing and natural drying are carried out, and AlPO4-34 molecular sieve raw powder is obtained. The method has the advantages that green effect, environment protection and economy are realized, the implementation condition is simple, and wide application prospects are realized.

The invention discloses a method for preparing a low-pour-point lubricant additive from low-priced cotton seed oil. The method comprises the following steps: mixing cotton seed oil, methanol and potassium hydroxide so as to prepare fatty acid methyl esters, uniformly mixing the fatty acid methyl esters, formic acid and petroleum ethers at room temperature, stirring and heating the obtained mixture, dripping a mixture of hydrogen peroxide and phosphoric acid into the obtained mixture, standing the obtained product to carry out delamination, separating a water layer, washing an oil layer by using water until the oil layer is neutral, and carrying out reduced pressure distillation to obtain colorless transparent oily epoxidized fatty acid methyl esters, wherein the epoxy value is greater than 4-7, the iodine value is less than 2-0, the acid value is less than 1, and the yield is 90-94%; adding calcium carbonate into a residual formic acid solution after reaction so as to obtain calcium formate which can be recycled; and carrying out esterification reaction on the epoxidized fatty acid methyl esters so as to obtain epoxidized fatty acid methyl ester mixed fatty acid esters. According to the method disclosed by the invention, atalyst application amount is low, the process is clean, the implementation conditions are simple, and the mass production can be implemented conveniently.

The invention discloses a pharmaceutic preparation of promotion of lactation for a puerperal. The pharmaceutic preparation is characterized in that raw materials for preparing the active ingredients of the preparation compriseangelica sinensis, semen sesami nigrum, colla corii asini, ginseng, astragalus mongholicus, tetrapanax papyriferus, corn stigma, uniflower swisscentaury root, trichosanthes kirilowii maxim, leonurus, dandelion, radix ophiopogonis and liquorice. According to the theory of traditional Chinese medicine and pharmacy, the qi and blood of a puerperal puerpera upwards move to generate the milk after the parturition, and the milk is the metaplasia of blood; qi runs, thus the puerperal puerpera is insufficient in milk due to weak qi and blood, and blocked channels of breast. According to the pharmaceutic preparation disclosed by the invention, various medicines are combined, so that source is provided for the milk, and the effects on replenishing qi, nourishing blood, promoting blood circulation to remove meridian obstruction, tonifying spleen and invigorating stomach, freeing channels of breast, alleviating water retention and promoting lactation, tonifying spleen and promoting lactation, and regulating the blood condition and producing milk.

The invention discloses an organic tin-inorganic tin hybrid Sn18 type crystalline tin-oxygen cluster compound and a preparation method thereof, and belongs to the field of inorganic chemistry. Substituted benzoic acid, phenylphosphonic acid, SnCl4. 5H2O and butylstannic acid are used as raw materials, acetonitrile, isopropanol and water are used as a mixed solvent, and three cases of organic tin-inorganic tin hybrid Sn18 type crystalline tin-oxygen cluster compounds are prepared through self-assembly reaction at 100 DEG C. The material disclosed by the invention has accurate structural information, high hydrophobicity and good stability, and is expected to be used as a novel tin-oxygen cluster material for preparing photoresist in an EUV (Extreme Ultraviolet) photoetching technology. The raw materials are easy to obtain, the preparation method is simple, the yield is high, and low cost and high benefit can be realized.

The invention provides a method of screening medicaments with high accuracy and high repeatability. The method comprises the following steps: 1) preparing a patterned fiber electrospinning receiving board, and preparing a receiving board with a patterned metal silver layer by utilizing a photoetching technology and a direct current magnetron sputtering technology; 2) preparing patterned electrospinning fibers, and carrying out electrostatic spinning on an object obtained in the step 1); 3) preparing a PDMS cavity; 4) connecting the objects obtained in the second and third steps by virtue of plasma treatment; and 5) inoculating primary mouse myocardial cells to the patterned electrospinning fibers in the object obtained in the step 4), pumping a culture medium into the cavity of the object obtained in the step 4) by virtue of an injection pump, then pumping the medicaments, recording the beating frequency of the myocardial cells within 20 days after the medicaments are pumped to obtain an EC50 value, and screening the medicaments according to the EC50 value. According to the method disclosed by the invention, normal growth of the cells in smaller cavity is realized, and the method also has the effects of screening the medicaments and reusing and is high in the accuracy and the repeatability.

The invention discloses an RLS adaptive filtering method for an open-type shock wave target scoring system, and solves the problems that a filtering frequency band is limited, the method is difficultto adapt to a complex environment and a reference signal of a noisy shock wave signal is difficult to obtain in the prior art. The method comprises the steps of collecting noisy projectile shock wavesignals; processing delay of noisy projectile shock wave signals; setting an adaptive filtering initial value; and updating the filter weight coefficient based on an RLS algorithm of the variable forgetting factor, and outputting the denoised shock wave signal. The invention further constructs an RLS adaptive filtering system which is sequentially connected with the delayer, the RLS adaptive filter and the differencing device. According to the invention, the delay signal of the noisy shock wave signal is used as the reference input of the adaptive filter, and the RLS adaptive filtering based on the variable forgetting factor is used for the signal processing of the shock wave target reporting system, so that the method has the advantages of simple implementation condition, adaptation to environmental change, high convergence speed and high precision. The device is used for an open-type shock wave target-scoring system.

A seed-directed fluorine-free synthetic method of AlPO4-34 is characterized in that relative molecular sieve crystal that is ground is used as seed crystal, the seed crystal is added into a mixture ofan aluminum source, a phosphorus source, an organic templating agent and water in the molar ratio of Al2O3:P2O5:R:H2O being 1.0:(0.8-1.0):(7.0-9.0):50; synthetic gel is made by uniform mixing and istransferred into a stainless steel kettle; hydrothermal crystallization is performed under 170-200 DEG C and self-generated pressure for 1-20 days; the crystalized material is cooled naturally to roomtemperature before conventional molecular sieve aftertreatment; cooling is performed before washing and drying to obtain the finished product.

The invention discloses a pluggable component data aggregation system and aggregation method based on multiple systems. According to the method, a convergence collector of a data convergence system isused to be adaptive to multiple data sources, multiple protocols and multiple interface data sources. A target data source is collected through a hot-pluggable convergence model device, collected data is converted into standard structured data through an intermediate data model conversion layer, data streams are stored in message middleware, and then the data streams are called from the message middleware to be analyzed and processed. The method does not need to collect the target data in modes such as code modification and plug-in addition in the collected service system, does not sense thecollected service system, has no performance influence and interference on the collection system, is quick in deployment, is simple in implementation condition, and is compatible with various operation systems and various system platforms.

The invention discloses a cultivating method for cordyceps militaris by using manyprickle acathopanax root and relates to a cultivating method for cordyceps militaris. The method is used for simplifying Chinese medicine compatibility dosage, increasing the utilization rate of cordyceps militaris and reducing the medicine consumption. The method comprises the following steps of: 1, activating strains; 2, preparing liquid strains; and 3, inoculating the liquid strains into a manyprickle acathopanax root solid culture medium for dark cultivation to obtain mycelia, then transferring to light and culturing until sporocarp grows up to 2 cm in height, after gas introduction, continuing culturing until the sporosarp grows up to 4-8 cm in height, yellow powdery substances appear on the surface of the sporosarp as well as small thorns appear on the top end, and harvesting. According to the method disclosed by the invention, active ingredients of the manyprickle acathopanax root are transferred into the sporocarp of cordyceps militaris, so that a beneficial curative effect of cordyceps militaris is indirectly enhanced, the method of compatibility of cordyceps militaris and manyprickle acathopanax root in traditional Chinese medical science is simplified, the utilization ratio, nutrition and medical value of cordyceps militaris are improved, the yield of cordyceps militaris is improved, the growth cycle of cordyceps militaris is shortened, and the quality of cordyceps militaris is improved; and moreover, implementing conditions are easily achieved.

The invention relates to the field of health-care foods, in particular to a Chuzhou flos chrysanthemi and cordyceps cicadae fermented beverage and a preparation method thereof. The preparation methodof the Chuzhou flos chrysanthemi and cordyceps cicadae fermented beverage comprises the following steps of (1) performing activated culture on cordyceps cicadae strains on a culture medium; (2) performing liquid fermentation culture on the treated cordyceps cicadae strains; (3) preparing a cordyceps cicadae liquid culture medium containing Chuzhou flos chrysanthemi, and performing fermentation culture on cordyceps cicadae; (4) adding other ingredients to the fermented Chuzhou flos chrysanthemi and cordyceps cicadae fermentation liquid, and performing uniform mixing; and (5) performing filling,performing sterilization, performing degassing and performing sealing and covering. The preparation method disclosed by the invention is simple to operate and short in cycle; the prepared Chuzhou flos chrysanthemi and cordyceps cicadae fermented beverage has fragrant smell, does not have specific bitterness of Chuzhou flos chrysanthemi, is rich in nutrients, and has the health-care efficacy of enhancing the immunity of human bodies, nourishing and strengthening bodies, nourishing the liver to improve visual acuity, resisting ageing, resisting viruses and the like. Besides, the diversity of cordyceps sobolifera and Chuzhou flos chrysanthemi products is enriched. In addition, the implementation conditions are easy to reach, and large-scale trade popularization can be performed.