Ceramic substrate and preparation method thereof, and power module
A technology of ceramic substrate and ceramic slurry, applied in ceramic layered products, chemical instruments and methods, layered products, etc., can solve the problems of high cost, application limitation, large thermal resistance, etc., and achieve high density and high strength. and the effect of toughness
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[0030] The present invention also provides a method for preparing the ceramic substrate, which includes the following steps: tape-casting to prepare the green body of the core layer, the green body of the upper transition layer, the green body of the lower transition layer, the green body of the upper surface layer and the green body of the lower surface layer; The order of upper surface layer-upper transition layer-core layer-lower transition layer-lower surface layer is to stack each green body successively, and after isostatic pressing, glue is discharged and sintered to obtain the ceramic substrate.
[0031] In the present invention, the method used to prepare the green body is tape casting, and the equipment and process conditions of the tape casting are well known to those skilled in the art. ceramic paste.
[0032] Specifically, the materials of the core layer and the transition layer of the ceramic substrate are both zirconia toughened alumina, therefore, the core laye...
Embodiment 1
[0045] (1) Preparation of ceramic slurry
[0046] Weigh Al according to the composition in Table 2 2 o 3 The required components of the slurry, ball mill ceramic powder, solvent and dispersant in a planetary ball mill for 4 hours, then add binder and plasticizer, ball mill for another 8 hours, add defoaming agent, finally ball mill for 1 hour, vacuum degassing for 0.5 hours h, that is, to get Al 2 o 3 slurry.
[0047] Weigh the required components of the ZTA10 slurry according to the components in Table 2, ball mill the ceramic powder, solvent and dispersant in a planetary ball mill for 4 hours, then add binder and plasticizer, ball mill for another 8 hours, and add defoaming agent agent, and finally ball milled for 1 hour, vacuum defoaming for 0.5 hours, and the ZTA10 slurry was obtained.
[0048] Weigh the required components of the ZTA10 slurry according to the components in Table 2, ball mill the ceramic powder, solvent and dispersant in a planetary ball mill for 4 ho...
Embodiment 2
[0055] Prepare ceramic slurry and ceramic green body according to the same method as in Example 1, and then prepare ceramic substrate S2 according to the following steps:
[0056] Cut the green body prepared in step (2) into 200mm×150mm, and then follow the green body Al 2 o 3 -Green ZTA10-Green ZTA20-Green ZTA10-Green Al 2 o3 Stack 5 layers of ceramic green bodies together in the following order; press the stacked ceramic green bodies with a warm water isostatic press, set the parameters of the warm water isostatic press at 85°C, and hold the pressure at 30MPa for 20min.
[0057] Finally, the pressed ceramic green body is put into a muffle furnace for debinding and sintering at one time. The debinding procedure is as follows: the temperature is raised from room temperature to 600°C at a rate of 0.5°C / min, and from room temperature to 600°C at a rate of 3°C / min. Raise the temperature from 600°C to 1600°C, hold at 1600°C for 3 hours, then cool down to 600°C at a rate of 8°C / m...
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