Preparation of styrene light diffusing agent
A light diffusing agent, styrene-based technology, applied in the field of preparation of styrene-based light diffusing agents, can solve the problems of agglomeration, poor dispersion of light diffusing agents, etc.
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Embodiment 1
[0023] Step 1. Preparation of water phase
[0024] Add 1000Kg of water and 1Kg of polyvinyl alcohol into a 2000L autoclave, and stir evenly.
[0025] Step 2. Preparation of oil phase
[0026] In a 500L reactor, 100Kg styrene, 4Kg divinylbenzene, 0.5Kg perfluoro-n-propyl vinyl ether, 0.3Kg hexafluoropropylene dimer, 0.4Kg 1-ethoxy-3-trifluoromethyl -1,3-butadiene, add 0.08Kg benzoyl peroxide, stir well.
[0027] Step 3. Polymerization
[0028] Add the oil phase solution prepared in the beaker in step 2 to the high-pressure reactor equipped with the prepared water phase in step 1, then react at 80°C for 14 hours, centrifuge after the reaction, and dry to obtain the product. The number is SX-1.
Embodiment 2
[0030] Step 1. Preparation of water phase
[0031] Add 1000Kg of water and 0.5Kg of polyvinyl alcohol into a 2000L autoclave, and stir evenly.
[0032] Step 2. Preparation of oil phase
[0033] In a 500L reactor, 100Kg styrene, 0.5Kg divinylbenzene, 0.1Kg perfluoro-n-propyl vinyl ether, 0.1Kg hexafluoropropylene dimer, 0.1Kg 1-ethoxy-3-trifluoromethane Base-1,3-butadiene, add 0.5Kg benzoyl peroxide, stir well.
[0034] Step 3. Polymerization
[0035] Add the oil phase solution prepared in the beaker in step 2 to the high-pressure reactor equipped with the prepared water phase in step 1, then react at 70°C for 20 hours, centrifuge after the reaction, and dry to obtain the product. The number is SX-2.
Embodiment 3
[0037] Step 1. Preparation of water phase
[0038] Add 1000Kg of water and 2Kg of polyvinyl alcohol into a 2000L autoclave, and stir evenly.
[0039] Step 2. Preparation of oil phase
[0040] In a 500L reactor, 100Kg styrene, 10Kg divinylbenzene, 1Kg perfluoro-n-propyl vinyl ether, 1Kg hexafluoropropylene dimer, 1Kg1-ethoxy-3-trifluoromethyl-1, 3-butadiene, add 2Kg benzoyl peroxide, stir well.
[0041] Step 3. Polymerization
[0042] Add the prepared oil phase solution in the beaker in step 2 to the high-pressure reactor equipped with the prepared water phase in step 1, then react at 90°C for 10 h, centrifuge after the reaction, and dry to obtain the product. The number is SX-3.
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