A composite foaming insulating material and a preparing method thereof
A thermal insulation material and composite foaming technology, which is applied in the field of thermal insulation building materials and its preparation, can solve the problems of complex process and high cost, and achieve the effects of low thermal conductivity, low cost and alleviating tire pollution
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Embodiment 1
[0018] Embodiment 1: Preparation of composite foam insulation material
[0019] (1) Weigh 90g of polyethylene glycol 4000 into a beaker, put it in an oil bath and heat it at 60°C until it melts, add 30g of rubber powder (60 mesh), 5g of polyethylene glycol 200, and 1g of surfactant dimethyl Silicone oil, stir evenly at constant temperature;
[0020] (2) Weigh 43g of 4,4'-diphenylmethane diisocyanate and dissolve it in 38g of dichloromethane, stir well, add to the mixing system in step (1), stir at a constant temperature for 25s, let the mixture freely foam and mature at 35°C 1h to obtain a composite foam insulation material.
[0021] The composite foam insulation material is measured according to GB / T6344-2008, and its tensile strength is
[0022] 134KPa. The thermal conductivity is 0.027W / (m K), and the bulk density is 63Kg / m 3 .
Embodiment 2
[0023] Embodiment 2: Preparation of composite foam insulation material
[0024] (1) Weigh 152g of polyethylene glycol 6000 into a beaker, put it in an oil bath and heat it at 75°C until it melts, add 40g of rubber powder (120 mesh), 8g of polyethylene glycol 400, and 1.2g of surfactant diethylene glycol Base silicone oil, stir evenly at constant temperature;
[0025] (2) Weigh 40g of 2,4'-diphenylmethane diisocyanate and dissolve it in 35g of n-pentane, stir well, add to the mixing system in step (1), stir at a constant temperature for 10s, let the mixture freely foam and mature at 28°C 30h to obtain a composite foam insulation material.
[0026] The composite foam insulation material is measured according to GB / T6344-2008, and its tensile strength is 142KPa. The thermal conductivity is 0.031W / (m K), and the bulk density is 66Kg / m 3 .
Embodiment 3
[0027] Embodiment 3: Preparation of composite foam insulation material
[0028] (1) Weigh 380g of polyethylene glycol 20000 into a beaker, put it in an oil bath and heat it at 95°C until it melts, add 200g of rubber powder (200 mesh), 105g of polyethylene glycol 600, and 4.5g of surfactant dimethyl Base silicone oil, stir evenly at constant temperature;
[0029] (2) Weigh 176g of 2,2'-diphenylmethane diisocyanate and dissolve it in 155g of cyclopentane, stir evenly, add to the mixing system in step (1), stir at a constant temperature for 15s, and let the mixture freely foam at 25°C, Aging for 48 hours to obtain a composite foam insulation material.
[0030] The composite foam insulation material is measured according to GB / T6344-2008, and its tensile strength is 125KPa. The thermal conductivity is 0.026W / (m K), and the bulk density is 68Kg / m 3 .
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