Modified bamboo pulp fiber wallpaper preparation method
A bamboo pulp fiber and modification technology, which is applied in the field of preparation of modified bamboo pulp fiber wallpaper, can solve the problems of antibacterial, poor burst resistance, unusable recycling, natural decomposition, easy to breed mold, etc., and achieve remarkable antibacterial effect
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example 1
[0020]First weigh 200g of bamboo pulp fiber, put it into a 1L Erlenmeyer flask, add 500mL of sodium periodate solution with a mass concentration of 60%, place it on a magnetic stirrer and stir at a speed of 300r / min for 10min, and add the mass concentration of Adjust the pH of 30% hydrochloric acid solution to 6, place it in a constant temperature box, and oxidize it in the dark at 30°C for 2 hours. After filtering, rinse the filter residue with glycerol and distilled water for 3 times, and dry it with a vacuum dryer to obtain oxidized bamboo pulp. fiber; then weigh 100g sericin, dissolve it in 400mL distilled water to obtain a sericin solution, immerse the oxidized bamboo pulp fiber prepared above into the sericin solution and move it into a water bath, heat up to 50°C, shake After bed shaking reaction for 2 hours, filter to obtain the filter residue, put the filter residue in an oven, keep it warm at 70°C for 5min, then raise the temperature to 150°C and bake for 3min to obta...
example 2
[0023] First weigh 250g of bamboo pulp fiber, put it into a 1L Erlenmeyer flask, add 550mL of sodium periodate solution with a mass concentration of 60%, place it on a magnetic stirrer and stir at a speed of 350r / min for 15min, and add the mass concentration of Adjust the pH of 30% hydrochloric acid solution to 6.5, place it in a constant temperature box, and oxidize it in the dark at 33°C for 2.5 hours. After filtering, wash the filter residue with glycerol and distilled water for 4 times, and dry it with a vacuum dryer to obtain oxidized bamboo. Pulp fiber; then weigh 150g sericin, dissolve it in 450mL distilled water to obtain a sericin solution, immerse the oxidized bamboo pulp fiber prepared above into the sericin solution and move it into a water bath device, heat up to 55°C, After oscillating on a shaking table for 2.5 hours, filter to obtain the filter residue, put the filter residue in an oven, keep it warm at 75°C for 8 minutes, and then heat up to 160°C for 4 minutes...
example 3
[0026] First weigh 300g of bamboo pulp fiber, put it into a 1L Erlenmeyer flask, add 600mL of sodium periodate solution with a mass concentration of 60%, place it on a magnetic stirrer and stir at a speed of 400r / min for 20min, and add the mass concentration of Adjust the pH of 30% hydrochloric acid solution to 7, place it in a constant temperature box, and oxidize it in the dark at 35°C for 3 hours. After filtering, rinse the filter residue with glycerol and distilled water for 5 times, and dry it with a vacuum dryer to obtain oxidized bamboo pulp. fiber; then weigh 200g sericin, dissolve it in 500mL distilled water to obtain a sericin solution, immerse the oxidized bamboo pulp fiber prepared above into the sericin solution and move it into a water bath, heat up to 60°C, shake After bed shaking reaction for 3 hours, filter to obtain the filter residue, put the filter residue in an oven, keep it warm at 80°C for 10min, then raise the temperature to 170°C and bake for 5min to ob...
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