Ethylene tetrapolymerization catalyst composition and ethylene tetrapolymerization method
A technology of ethylene tetramerization and composition, which is applied in the field of ethylene tetramerization catalyst composition and ethylene tetramerization, can solve the problems of high cost, high production cost, and harsh process requirements, and achieve high polymerization activity and rapid reaction initiation , good repeatability
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Embodiment 1
[0034] A 300mL stainless steel polymerization kettle was used. The autoclave was heated to 80°C, evacuated and replaced with nitrogen for several times, then filled with ethylene for replacement once, and lowered to the set temperature. Aqueous methylcyclohexane was added at 40°C, followed by 1 μmol of bisphosphine ligand (where R 1 is methyl, R 2 is ethyl, R 3 , R 4 , R 5 and R 6 All are phenyl), 1 μmol of chromium trichloride, quantitative cocatalyst triethylaluminum, the total volume of the mixed solution is 100mL, based on the weight of the organic solvent, the weight content of water is 5ppm, the moles of aluminum and chromium The ratio is 300. The reaction pressure was controlled at 4.0 MPa, and ethylene was introduced to carry out ethylene tetramerization. After 0.5 hours of reaction, the system was cooled to room temperature, the gas phase product was collected in a gas metering tank, and the liquid phase product was collected in a conical flask, and gas chromat...
Embodiment 2
[0037] Same as Example 1, the difference is that the weight content of water is 30 ppm. See Table 1 for the data.
Embodiment 3
[0039] Same as Example 1, the difference is that the weight content of water is 50 ppm. See Table 1 for the data.
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