Technology for producing peony seed oil
A peony seed oil and production process technology, applied in the direction of fat oil/fat production, fat production, fat oil/fat refining, etc., can solve the problems of low oil yield, low utilization rate of peony seed nutrients, low extraction rate, etc. To achieve the effect of improving utilization rate, shortening extraction time and improving extraction rate
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Embodiment 1
[0029] A production process of peony seed oil, comprising the following steps:
[0030] (1) Peony seeds are peeled from the peony pods, dried for 6-12 hours under the condition of vacuum degree of 0.08~0.09MPa negative pressure and temperature of 23~26°C, and then crushed into peony seed powder , the water mass content of peony seed powder is 9~10%;
[0031] (2) Put the dried peony seed powder into a Soxhlet extraction device, add a mixture of extraction agents ethyl acetate, ethanol and petroleum ether, the volume ratio of ethyl acetate, ethanol and petroleum ether is 1:3: 8. The liquid-solid ratio of the mixture of ethyl acetate, ethanol and petroleum ether to the peony seed powder is 12ml / g, soak for 2 hours, and then extract at a temperature of 92°C for 2 hours to obtain a crude extract containing peony seed oil liquid;
[0032] (3) concentrating the crude extract containing peony seed oil under reduced pressure, recovering ethyl acetate, ethanol and petroleum ether, and...
Embodiment 2
[0040] A production process of peony seed oil, comprising the following steps:
[0041] (1) Peony seeds are peeled from the peony pods, dried for 6-12 hours under the condition of a vacuum of 0.08-0.09MPa negative pressure and a temperature of 20-30°C, and then crushed into peony seed powder , the water mass content of peony seed powder is 9~10%;
[0042] (2) Put the dried peony seed powder into a Soxhlet extraction device, add a mixture of extraction agents ethyl acetate, ethanol and petroleum ether, the volume ratio of ethyl acetate, ethanol and petroleum ether is 1:4: 7. The liquid-solid ratio of the mixture of ethyl acetate, ethanol and petroleum ether to the peony seed powder is 10ml / g, soak for 2 hours, and then extract at a temperature of 95°C for 2 hours to obtain a crude extract containing peony seed oil liquid;
[0043] (3) concentrating the crude extract containing peony seed oil under reduced pressure, recovering ethyl acetate, ethanol and petroleum ether, and ob...
Embodiment 3
[0051] A production process of peony seed oil, comprising the following steps:
[0052] (1) Peony seeds are peeled from the peony pods, dried for 6-12 hours under the condition of a vacuum of 0.08-0.09MPa negative pressure and a temperature of 20-30°C, and then crushed into peony seed powder , the water mass content of peony seed powder is 9~10%;
[0053] (2) Put the dried peony seed powder into a Soxhlet extraction device, add a mixture of extraction agents ethyl acetate, ethanol and petroleum ether, the volume ratio of ethyl acetate, ethanol and petroleum ether is 1:2: 9. The liquid-solid ratio of the mixture of ethyl acetate, ethanol and petroleum ether to the peony seed powder is 15ml / g, first soak for 1h, and then extract at a temperature of 90°C for 1.5h to obtain crude peony seed oil. Extraction solution;
[0054] (3) concentrating the crude extract containing peony seed oil under reduced pressure, recovering ethyl acetate, ethanol and petroleum ether, and obtaining p...
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