Method for preparing high-purity silicon by energy-saving and environmental protection technology
An energy-saving, environmentally-friendly, high-tech technology, applied in chemical instruments and methods, silicon compounds, sustainable manufacturing/processing, etc., can solve the problems of complex production process, high production cost, and many reaction steps, and achieve simple production process , Low production cost and simple structure
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Embodiment 1
[0030] A method for producing high-purity silicon by utilizing energy-saving and environment-friendly technologies, comprising the following steps in sequence:
[0031] (1) Mix white carbon black and LiH uniformly in a ratio of 1.0094:1.4517 parts by weight to obtain a mixture, and place the mixture in a heating furnace with a chamber volume of 20 liters;
[0032] (2) Evenly spread 200-mesh carbon powder on the surface of the mixture, and the ratio of carbon powder to the mixture is 0.2161:2.4611 by weight;
[0033] (3) The temperature of the furnace cavity of the heating furnace is raised to 240°C through 0.8h, and the temperature is kept for 1.4h;
[0034] (4) The temperature of the furnace cavity of the heating furnace is raised to 360°C through 0.8h, and the temperature is kept for 4.2h to obtain the reaction product;
[0035] (5) cooling the reaction product to room temperature, washing it three times with normal temperature distilled water, each time using 20 parts by w...
Embodiment 2
[0039] A method for producing high-purity silicon by utilizing energy-saving and environment-friendly technologies, comprising the following steps in sequence:
[0040] (1) Quartz sand, LiAlH 4 Mix evenly according to the ratio of 0.8909:1.3501 parts by weight to obtain a mixture, and place the mixture in a heating furnace with a chamber volume of 10 liters;
[0041] (2) Evenly spread 140-mesh carbon powder on the surface of the mixture, and the ratio of carbon powder to the mixture is 0.1859:2.241 by weight;
[0042] (3) The temperature of the furnace cavity of the heating furnace is raised to 200° C. over 0.5 h, and the temperature is kept for 2 h;
[0043] (4) The temperature of the furnace chamber of the heating furnace is raised to 300° C. over 0.5 h, and the temperature is kept for 6 h to obtain the reaction product;
[0044] (5) cooling the reaction product to room temperature, washing it three times with normal temperature distilled water, each time using 15 parts by...
Embodiment 3
[0048] A method for producing high-purity silicon by utilizing energy-saving and environment-friendly technologies, comprising the following steps in sequence:
[0049] (1) White carbon black, NaBH 4 Mix evenly in the ratio of 0.9092:1.4078 parts by weight to obtain a mixture, and place the mixture in a heating furnace with a chamber volume of 15 liters;
[0050] (2) Evenly spread 170 mesh carbon powder on the surface of the mixture, the ratio of carbon powder to the mixture is 0.2103:2.317 by weight;
[0051] (3) The temperature of the furnace cavity of the heating furnace is raised to 220° C. over 0.65 hours, and kept for 1.7 hours;
[0052] (4) The temperature of the furnace chamber of the heating furnace is raised to 330°C through 0.65h, and the temperature is kept for 5h to obtain the reaction product;
[0053] (5) cooling the reaction product to room temperature, washing it three times with normal temperature distilled water, each time using 18 parts by weight of norma...
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