Downhole drilling crosslinked gel leak stopping agent and leak stopping method thereof
A technology of cross-linked gel and plugging agent, which is applied in wellbore/well components, chemical instruments and methods, earthwork drilling and production, etc. It can solve the problems of high-strength plugging, high-strength plugging difficulty, low gel breaking pressure, and plugging Failure and other problems, to achieve the effect of improving plugging effect and firm rate, overcoming low compressive strength, and preventing mud leakage
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Embodiment 1
[0019] This embodiment provides a cross-linked gel plugging agent for drilling downhole. The plugging agent includes: 25% polyacrylamide, 25% organic amines, sugarcane Slag 25%, polyvinyl alcohol 5%, sodium bentonite 20%.
[0020] The lost circulation agent is prepared by uniformly mixing the above components in proportion.
[0021] To simulate downhole cross-linking plugging, add the above plugging agent into 100mL of clean water, stir evenly, and solidify at 100°C for 4 hours; at 120°C for 2 hours; at 150°C for 2 hours.
[0022] It can be seen that the higher the temperature, the shorter the curing time; when the temperature is above 120°C, the curing time tends to be consistent. However, the cross-linking time of conventional cross-linked lost circulation plugging agents has nothing to do with temperature, and is basically completed within 1 hour. At the same time, the strength after crosslinking is weaker than that of the lost circulation agent of this embodiment.
Embodiment 2
[0024] This embodiment provides a cross-linked gel plugging agent for drilling downhole. The plugging agent includes: 22.5% polyacrylamide, 22.5% aldehyde compounds, organic Acid 9%, walnut shell 22.5%, PET 4.5%, sodium bentonite 18%.
[0025] The lost circulation agent is prepared by uniformly mixing the above components in proportion.
[0026] When simulating downhole cross-linking plugging, add the above plugging agent into 100mL of clean water, stir evenly, and solidify at 100°C for 2 hours; at 120°C for 1.5 hours; at 150°C for 1 hour. Compared with Example 1, the addition of coagulant organic acid shortens the curing molding time at the same temperature.
Embodiment 3
[0028] This embodiment provides a cross-linked gel plugging agent for downhole drilling. Based on the weight percentage of the plugging agent as 100%, the plugging agent includes: polyacrylamide 21%, organic amine 21%, organic acid 16.5%, sawdust 21%, polyvinyl alcohol 4%, sodium bentonite 16.5%.
[0029] The lost circulation agent is prepared by uniformly mixing the above components in proportion.
[0030] When simulating downhole cross-linking plugging, add the above plugging agent into 100mL of clean water, stir well, and solidify at 100°C for 1.5 hours; at 120°C for 75 minutes; at 150°C for 1 hour. Compared with Example 2, the amount of coagulant organic acid increases, and the curing molding time is shorter at the same temperature.
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