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Preparation method of rare earth load antibacterial agent

An antibacterial agent and rare earth technology, which is applied in the field of preparation of rare earth-loaded antibacterial agents, can solve problems such as easy loss, unstable antibacterial and antifungal properties, uneven distribution of rare earth elements, etc.

Inactive Publication Date: 2016-10-12
王金明
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The rare earth antibacterial agents prepared by the existing known technology are all ion exchange or compounding, the distribution of rare earth elements is uneven, easy to lose, and the antibacterial and antifungal properties are unstable

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] In a 500L reactor, add Q high-flow rate agarose microspheres and disperse them in ethanol according to the following ratio, and add bis(tricarbonylcyclopentadienyl molybdenum), 1-allyl-3-methyl chloride according to the following ratio Use imidazole, benzoyl peroxide, polyvinyl alcohol, sodium dodecylbenzenesulfonate, etc., heat up, and react at 80°C for 6 hours to obtain rare earth-containing Q high-flow agarose microsphere microsuspension liquid product, number M-1.

[0023] Component Kg

[0024] QHigh Flow Agarose Beads 10

[0025] Bis(tricarbonyl cyclopentadiene molybdenum) 2

[0026] 1-allyl-3-methyl imidazole chloride 0.3

[0027] Benzoyl peroxide 0.02

[0028] Polyvinyl alcohol 0.2

[0029] Sodium dodecylbenzenesulfonate 0.2

[0030] Ethanol 200

Embodiment 2

[0032] In a 500L reactor, add Q high-flow rate agarose microspheres and disperse them in ethanol according to the following ratio, and add bis(tricarbonylcyclopentadienyl molybdenum), 1-allyl-3-methyl chloride according to the following ratio Use imidazole, benzoyl peroxide, polyvinyl alcohol, sodium dodecylbenzenesulfonate, etc., heat up, and react at 70°C for 10 hours to obtain rare earth-containing Q high-flow agarose microsphere microsuspension liquid product, number M-2.

[0033] Component Kg

[0034] QHigh Flow Agarose Beads 5

[0035] Bis(tricarbonyl cyclopentadiene molybdenum) 1

[0036] 1-allyl-3-methyl imidazole chloride 0.1

[0037] Benzoyl peroxide 0.01

[0038] Polyvinyl alcohol 0.1

[0039] Sodium dodecylbenzenesulfonate 0.1

[0040] Ethanol 200

Embodiment 3

[0042] In a 500L reactor, add Q high-flow rate agarose microspheres and disperse them in ethanol according to the following ratio, and add bis(tricarbonylcyclopentadienyl molybdenum), 1-allyl-3-methyl chloride according to the following ratio Use imidazole, benzoyl peroxide, polyvinyl alcohol, sodium dodecylbenzenesulfonate, etc., heat up, and react at 60°C for 15 hours to obtain rare earth-containing Q high-flow agarose microsphere microsuspension Liquid product, number M-3

[0043] Component Kg

[0044] QHigh Flow Agarose Beads 15

[0045] Bis(tricarbonylcyclopentadienyl molybdenum) 3

[0046] 1-allyl-3-methyl imidazole chloride 0.5

[0047] Benzoyl peroxide 0.05

[0048] Polyvinyl alcohol 0.5

[0049] Sodium dodecylbenzenesulfonate 0.5

[0050] Ethanol 200

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PUM

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Abstract

The invention relates to a preparation method of a rare earth-loaded antibacterial agent. A certain amount of Q high-flow rate agarose microspheres is dispersed into ethanol, and bis(pentamethylcobalt cyclopentadiene), 1-allyl-3- Methyl imidazole chloride is subjected to a polymerization reaction to obtain a rare earth-containing Q high-flow agarose microsphere microsuspension product.

Description

technical field [0001] The invention relates to a preparation method of an antibacterial agent, in particular to a preparation method of a rare earth loaded antibacterial agent. Background technique [0002] Rare earth elements and their compounds have good anti-inflammatory, bactericidal, anti-cancer, anti-coagulation, and analgesic effects. Heterocyclic compounds are a class of compounds with a wide range of biological activities. Many heterocyclic compounds have biological activities such as sterilization, anti-inflammation, and anti-virus, so they have attracted much attention. After the heterocyclic compound forms a complex with metal ions, the antibacterial effect of the metal complex will be enhanced due to the synergistic effect. Relevant studies have shown that compared with many organic synthetic drugs, rare earth complexes have lower toxicity, and at the same time, no accumulation in the body has been found through oral or external use of rare earth complexes, so...

Claims

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Application Information

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IPC IPC(8): A01N55/02A01N43/50A01N25/10A01P1/00A01P3/00
CPCA01N55/02A01N25/10A01N43/50
Inventor 王琪宇王新
Owner 王金明
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