A kind of nano-silver antibacterial material and preparation method thereof
A nano-silver antibacterial and nano-silver particle technology, which is applied to nano-silver antibacterial materials and the preparation field of the above-mentioned nano-silver antibacterial materials, can solve problems such as the preparation process of nano-silver composite materials and the limited mechanical strength of nano-silver composite materials, and achieve Improved antibacterial stability, less environmental impact, and improved mechanical properties
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Embodiment 1
[0038] By weight, the nano-silver antibacterial material of the present embodiment comprises the following components:
[0039]
[0040] The preparation method of nano-silver antibacterial material in the present embodiment comprises the following steps:
[0041] (1) Preparation of Dialdehyde Sodium Alginate
[0042] Dissolve sodium alginate and sodium periodate in deionized water at a weight ratio of 1:0.1, and react in the dark for 6 hours at room temperature. The product is precipitated with ethanol, washed and dried in a vacuum environment at 35°C to obtain dialdehyde alginic acid sodium;
[0043] (2) Preparation of nano-silver particles-dialdehyde sodium alginate-casein composite material
[0044] Dissolve dialdehyde sodium alginate, casein, and silver nitrate in deionized water, and stir evenly to form a premixed solution. During this process, dialdehyde sodium alginate and casein undergo a cross-linking reaction, and at the same time, silver ions are The premixed ...
Embodiment 2
[0053] By weight, the nano-silver antibacterial material of the present embodiment comprises the following components:
[0054]
[0055] The preparation method of nano-silver antibacterial material in the present embodiment comprises the following steps:
[0056] (1) Preparation of Dialdehyde Sodium Alginate
[0057] Dissolve sodium alginate and sodium periodate in deionized water at a weight ratio of 1:0.5, and react in the dark for 24 hours at room temperature. The product is precipitated with acetone, washed and dried in a vacuum environment at 50°C to obtain dialdehyde alginic acid sodium;
[0058] (2) Preparation of nano-silver particles-dialdehyde sodium alginate-casein composite material
[0059] Dissolve dialdehyde sodium alginate, casein, and silver nitrate in deionized water, and stir evenly to form a premixed solution. During this process, dialdehyde sodium alginate and casein undergo a cross-linking reaction, and at the same time, silver ions are The premixed...
Embodiment 3
[0067] By weight, the nano-silver antibacterial material of the present embodiment comprises the following components:
[0068]
[0069]
[0070] The preparation method of nano-silver antibacterial material in the present embodiment comprises the following steps:
[0071] (1) Preparation of Dialdehyde Sodium Alginate
[0072] Dissolve sodium alginate and sodium periodate in deionized water at a weight ratio of 1:0.3, and react in the dark for 10 hours at room temperature. The product is precipitated with ether, washed and dried in a vacuum environment at 45°C to obtain dialdehyde alginic acid sodium;
[0073] (2) Preparation of nano-silver particles-dialdehyde sodium alginate-casein composite material
[0074] Dissolve dialdehyde sodium alginate, casein, and silver nitrate in deionized water, and stir evenly to form a premixed solution. During this process, dialdehyde sodium alginate and casein undergo a cross-linking reaction, and at the same time, silver ions are Th...
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