Granular material and preparation method thereof
A technology of pellets and carcass, applied in the field of superhard materials, which can solve problems such as complex equipment, easy fall-off of the carcass, and environmental pollution
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[0115] The present invention also provides a method for preparing the pellets, the method comprising the steps of:
[0116] 1) provide the carcass, wherein,
[0117] The carcass is prepared as follows: mix and disperse the carcass powder and the carcass forming agent evenly, and optionally press and embed the superhard core material into the center of the homogeneous mixture formed by the carcass powder and the carcass forming agent , forming the carcass;
[0118] Typically, the carcass powder includes (but not limited to): tungsten carbide powder, nickel powder, cobalt powder, manganese powder, copper-tin alloy powder, iron powder, copper powder, zinc powder, silver powder, tungsten powder, Molybdenum powder, silicon carbide powder, silicon nitride powder, alumina, boron powder, ceramic powder, or a combination thereof;
[0119] Typically, the carcass forming agent includes (but not limited to): rubber, silicone rubber, or a combination thereof;
[0120] Representatively, ...
Embodiment 1
[0168] Example 1 Pellet 1
[0169] The tungsten carbide powder, nickel powder, cobalt powder, manganese powder, and copper-tin-10 powder are uniformly mixed in the weight ratio of 50:12:16:8:32. The mixed powder and methyl vinyl silicone rubber were uniformly mixed on an open mill to form a carcass material in which the mixed powder accounted for 93wt%, the rotating speed was 35r / min, and the time was 15min. Take 0.0474g of carcass material, press and embed diamonds with a single particle diameter of 450 μm and a boron-coated layer into the carcass material to form a carcass. The carcass was shaped, and then placed in a vacuum high-temperature furnace for sintering at a sintering temperature of 780° C. and a holding time of 60 minutes to obtain pellets 1 .
[0170] result
[0171] The particle size, bonding performance, etc. of the obtained pellets were measured.
[0172] figure 1 is a photograph of pellet 1 prepared in Example 1. From figure 1 It can be obtained that th...
Embodiment 2
[0174] Example 2 pellet 2
[0175] The tungsten carbide powder, nickel powder, cobalt powder, manganese powder, and copper tin-15 powder are uniformly mixed in the weight ratio of 55:13:18:9:36. The mixed powder and methyl vinyl silicone rubber were evenly mixed on an open mill to form a carcass material in which the mixed powder accounted for 85 wt%, with a rotating speed of 30 r / min and a time of 10 min. Take 0.0116g of carcass material, press and embed diamonds with a single particle diameter of 400 μm and a chrome-plated layer on the surface of the carcass material to form a carcass. The carcass was shaped, and then placed in a vacuum high-temperature furnace for sintering at a sintering temperature of 750° C. and a holding time of 40 minutes to obtain pellets 2 .
[0176] result
[0177] The particle size of the obtained granules is 0.9mm, and the powder does not fall off after being ultrasonicated in water for 10 minutes.
[0178] Example 3 Pellet 3
[0179]The tungs...
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Abstract
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