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Method for converting nano graphite into one-dimensional carbon nano fiber by laser irradiation

A carbon nanofiber and nanographite technology, applied in the chemical characteristics of fibers, textiles and papermaking, etc., can solve the problems of polluted environment, long manufacturing cycle, small output and difficult continuous growth, etc., to avoid environmental pollution and save manpower and material resources.

Inactive Publication Date: 2016-10-26
ZHEJIANG COLLEGE OF ZHEJIANG UNIV OF TECHOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The carbon nanofibers prepared by the chemical vapor deposition method have a large diameter, and the yield is small, it is difficult to grow continuously and accompanied by a certain amount of carbon black; the carbon nanofibers prepared by the flame method are difficult to control the shape and arrangement of the carbon nanofibers; the electrospinning method The carbon nanofiber skin-core structure is serious, the mechanical properties are poor, and the surface is rough
At the same time, the preparation conditions of these processes are relatively harsh, such as the need to add catalysts, the preparation temperature is difficult to control, the production cycle is long, accompanied by the formation of additional products, polluting the environment, etc.

Method used

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  • Method for converting nano graphite into one-dimensional carbon nano fiber by laser irradiation
  • Method for converting nano graphite into one-dimensional carbon nano fiber by laser irradiation
  • Method for converting nano graphite into one-dimensional carbon nano fiber by laser irradiation

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Embodiment 1

[0042] Such as figure 1 As shown, a method for converting one-dimensional carbon nanofibers into one-dimensional carbon nanofibers by laser irradiation of nano-graphite in this embodiment comprises the following steps: figure 2 as shown, figure 2 It is a schematic diagram of an experimental device for transforming one-dimensional carbon nanofibers into one-dimensional carbon nanofibers by laser irradiation of the present invention; it mainly includes a computer 1, the computer 1 is connected to the laser 2, and the laser 2 and the airtight container 3 are scanned The vibrating mirror 4 provides an angle of vertical incidence; the airtight container 3 is also installed with a protective atmosphere device 5;

[0043]1) According to the melting point of graphite, material properties, phase transition temperature, graphite size, (the physical parameters of nano-graphite are shown in Table 1, and Table 1 is the physical parameter table of nano-graphite of the present embodiment)...

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Abstract

The invention discloses a method for converting nano graphite into one-dimensional carbon nano fiber by laser irradiation, comprising the following steps: 1), selecting a laser energy density reference value according to conversion physical parameters of nano graphite, selecting a laser through the laser energy density reference value, and setting laser process parameters; 2), using the data of step 1) to acquire an optimal laser energy density set value of a one-dimensional carbon nano wire, selecting reasonable laser process parameters by using the optimal laser energy density set value, and using a protective gas to prevent graphite oxidation so as to produce one-dimensional nano carbon fiber; the carbon nano fiber is controllably industrialized; the defects due to chemical methods and other methods are avoided; no waste is caused ,and manpower and material resources are saved.

Description

technical field [0001] The invention relates to a method for transforming one-dimensional carbon nanofibers by laser irradiation of nanometer graphite. Background technique [0002] Carbon is one of the most common and important elements on the earth. For a long time, people believed that there are only two forms of carbon: graphite and diamond. Since Smalley discovered fullerene in 1985 and Juno Iijima discovered carbon nanotubes in 1991, carbon nanomaterials have attracted extensive attention for their excellent electrical, magnetic, optical and mechanical properties. , biosensing and other fields have been widely used. The unique structure and excellent performance make it have many potential application values. [0003] So far, carbon nanomaterials with various shapes and structures have been prepared by various methods, such as carbon nanotubes, graphite nanocones, hollow carbon spheres, carbon nanocapsules, carbon nanorods, carbon nanoneedles, carbon nano fiber. An...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F9/12
CPCD01F9/12
Inventor 骆芳王为彬杨高林陆潇晓袁林江
Owner ZHEJIANG COLLEGE OF ZHEJIANG UNIV OF TECHOLOGY
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