Unlock instant, AI-driven research and patent intelligence for your innovation.

Preparation of a magnetic extreme pressure antiwear agent and energy-saving and environment-friendly engine oil containing the magnetic extreme pressure antiwear agent

An extreme pressure antiwear agent, energy saving and environmental protection technology, applied in the field of engine lubricants, can solve the problems of catalyst poisoning, reduction of catalytic effect, poisoning and failure of redox catalyst, etc., achieve good antiwear performance and improve wear resistance

Active Publication Date: 2020-07-17
SHANDONG YUANGEN PETROLEUM CHEM
View PDF4 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Due to the setting of exhaust emission requirements, it directly promotes the development of engine hardware technology. The development and changes of these hardware directly put forward new requirements for lubricating oil. The use of some metal elements that are easy to generate ash, such as Zn, has been limited; the redox device requires reducing the sulfur content, because sulfur is easy to poison the redox catalyst and fail, and because the engine burns lubricating oil, the sulfur content of lubricating oil The higher it is, the more carbon deposits will be burned, and the more sulfur-containing substances will be emitted; devices such as NOx removal devices, three-way catalysis, and selective reduction catalysis are also required to reduce the content of sulfur and phosphorus, because phosphorus will affect the three-way catalytic conversion. The impact of the catalyst poisons the catalyst, thereby reducing the catalytic effect. At the same time, through the analysis of the combustion products adhering to the valve, it is found that its main component is Ca 3 (PO 4 ) 2 , it is not only the product of gasoline engine combustion, which is a component of engine lubricating oil, but these combustion products often cause abnormal combustion such as surface ignition

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Preparation of a magnetic extreme pressure antiwear agent and energy-saving and environment-friendly engine oil containing the magnetic extreme pressure antiwear agent
  • Preparation of a magnetic extreme pressure antiwear agent and energy-saving and environment-friendly engine oil containing the magnetic extreme pressure antiwear agent

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] This embodiment provides a preparation method of a magnetic extreme pressure antiwear agent, and an energy-saving and environment-friendly engine oil containing the magnetic extreme pressure antiwear agent.

[0033] A preparation method of a magnetic extreme pressure antiwear agent, specifically comprising the following steps:

[0034] a. Graphene oxide modified with 140mg dodecylamine, 580mgFeCl 2 · 6H 2 O and 2mg of sodium acetate were dissolved in 55mL of ethylene glycol, and stirred evenly to obtain solution A;

[0035] b. Transfer solution A to an autoclave for reaction, the reaction temperature is 170°C, and the reaction time is 15 hours. After the reaction is completed, cool to room temperature to obtain solution B;

[0036] C, utilize magnet to do separation processing to solution B again, obtain reaction product A and reaction solution;

[0037] d. Washing the reaction product A successively with ultrapure water and anhydrous and alcohol-free for 6 times to ...

Embodiment 2

[0041] This embodiment provides a preparation method of a magnetic extreme pressure antiwear agent, and an energy-saving and environment-friendly engine oil containing the magnetic extreme pressure antiwear agent.

[0042] A preparation method of a magnetic extreme pressure antiwear agent, specifically comprising the following steps:

[0043] a, 150mg dodecylamine modified graphene oxide, 600mgFeCl 2 · 6H 2O and 3mg of sodium acetate were dissolved in 60mL of ethylene glycol, and stirred evenly to obtain solution A;

[0044] b. Transfer solution A to an autoclave for reaction, the reaction temperature is 180°C, and the reaction time is 16 hours. After the reaction is completed, cool to room temperature to obtain solution B;

[0045] C, utilize magnet to do separation processing to solution B again, obtain reaction product A and reaction solution;

[0046] d, the reaction product A was washed 8 times with ultrapure water and anhydrous and alcohol-free successively to obtain ...

Embodiment 3

[0050] a. Graphene oxide modified with 160mg dodecylamine, 650mgFeCl 2 · 6H 2 O and 4mg of sodium acetate were dissolved in 65mL of ethylene glycol, and stirred evenly to obtain solution A;

[0051] b. Transfer solution A to an autoclave for reaction, the reaction temperature is 190°C, and the reaction time is 17 hours. After the reaction is completed, cool to room temperature to obtain solution B;

[0052] C, utilize magnet to do separation processing to solution B again, obtain reaction product A and reaction solution;

[0053] d. The reaction product A was washed 12 times with ultrapure water and anhydrous and alcohol-free successively to obtain the reaction product B;

[0054] e. Finally, dry the reaction product B at a temperature of 50°C to obtain the final product, namely the magnetic extreme pressure antiwear agent;

[0055] An energy-saving and environment-friendly engine oil utilizing the above-mentioned magnetic extreme-pressure anti-wear agent, specifically comp...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention belongs to the field of engine lubricants, and relates to preparation of a magnetic extreme pressure anti-wearing additive and energy-saving environmental-friendly engine oil containing same. Preparation of the magnetic extreme pressure anti-wearing additive comprises the following steps: dissolving dodecylamine modified graphene oxide, FeCl2.6H2O and sodium acetate into ethylene glycol, uniformly stirring, transferring into a stainless steel high-pressure reaction kettle for reaction, cooling to the room temperature, separating a reaction product from a reaction solution by using a magnet, washing for multiple times with ultrapure water and absolute ethyl alcohol in sequence, and finally drying for later use. The energy-saving environmental-friendly engine oil containing the magnetic extreme pressure anti-wearing additive comprises basic oil, an anti-wearing agent, the magnetic extreme pressure anti-wearing additive, a high-temperature antioxidant, a clearing agent, a dispersing agent, a viscosity index improver, and the like. The engine oil designed from the magnetic extreme pressure anti-wearing additive is relatively good in bearing capability and extreme pressure anti-wearing property, and is relatively good in environmental-friendliness.

Description

technical field [0001] The invention belongs to the field of engine lubricants, and in particular relates to the preparation of a magnetic extreme pressure antiwear agent and energy-saving and environment-friendly engine oil containing the magnetic extreme pressure antiwear agent. Background technique [0002] Lubricating grease is one of the important supporting materials for modern transportation, modern industry and national defense industry. However, according to the survey of the United Nations Environmental Protection Organization, 50% of the air pollution in large and medium-sized cities comes from the exhaust emissions of fuel vehicles. Therefore, how to effectively control vehicle exhaust Emissions, to prevent the recurrence of the national heavy smog in early 2013, is the key to protecting the atmospheric environment on which we live. [0003] As we all know, automobile exhaust emissions contain many substances harmful to the ecological environment and human health...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C10M159/12C10M169/04C10N30/06C10N30/12C10N40/25H01F1/01
CPCC10M159/12C10M169/048C10M2205/022C10M2205/024C10M2215/064C10M2219/044C10M2223/045C10N2030/06C10N2030/12C10N2040/25H01F1/01C10N2010/04
Inventor 何茂伟袁俊洲徐金玲乔良
Owner SHANDONG YUANGEN PETROLEUM CHEM