Preparation of a magnetic extreme pressure antiwear agent and energy-saving and environment-friendly engine oil containing the magnetic extreme pressure antiwear agent
An extreme pressure antiwear agent, energy saving and environmental protection technology, applied in the field of engine lubricants, can solve the problems of catalyst poisoning, reduction of catalytic effect, poisoning and failure of redox catalyst, etc., achieve good antiwear performance and improve wear resistance
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Embodiment 1
[0032] This embodiment provides a preparation method of a magnetic extreme pressure antiwear agent, and an energy-saving and environment-friendly engine oil containing the magnetic extreme pressure antiwear agent.
[0033] A preparation method of a magnetic extreme pressure antiwear agent, specifically comprising the following steps:
[0034] a. Graphene oxide modified with 140mg dodecylamine, 580mgFeCl 2 · 6H 2 O and 2mg of sodium acetate were dissolved in 55mL of ethylene glycol, and stirred evenly to obtain solution A;
[0035] b. Transfer solution A to an autoclave for reaction, the reaction temperature is 170°C, and the reaction time is 15 hours. After the reaction is completed, cool to room temperature to obtain solution B;
[0036] C, utilize magnet to do separation processing to solution B again, obtain reaction product A and reaction solution;
[0037] d. Washing the reaction product A successively with ultrapure water and anhydrous and alcohol-free for 6 times to ...
Embodiment 2
[0041] This embodiment provides a preparation method of a magnetic extreme pressure antiwear agent, and an energy-saving and environment-friendly engine oil containing the magnetic extreme pressure antiwear agent.
[0042] A preparation method of a magnetic extreme pressure antiwear agent, specifically comprising the following steps:
[0043] a, 150mg dodecylamine modified graphene oxide, 600mgFeCl 2 · 6H 2O and 3mg of sodium acetate were dissolved in 60mL of ethylene glycol, and stirred evenly to obtain solution A;
[0044] b. Transfer solution A to an autoclave for reaction, the reaction temperature is 180°C, and the reaction time is 16 hours. After the reaction is completed, cool to room temperature to obtain solution B;
[0045] C, utilize magnet to do separation processing to solution B again, obtain reaction product A and reaction solution;
[0046] d, the reaction product A was washed 8 times with ultrapure water and anhydrous and alcohol-free successively to obtain ...
Embodiment 3
[0050] a. Graphene oxide modified with 160mg dodecylamine, 650mgFeCl 2 · 6H 2 O and 4mg of sodium acetate were dissolved in 65mL of ethylene glycol, and stirred evenly to obtain solution A;
[0051] b. Transfer solution A to an autoclave for reaction, the reaction temperature is 190°C, and the reaction time is 17 hours. After the reaction is completed, cool to room temperature to obtain solution B;
[0052] C, utilize magnet to do separation processing to solution B again, obtain reaction product A and reaction solution;
[0053] d. The reaction product A was washed 12 times with ultrapure water and anhydrous and alcohol-free successively to obtain the reaction product B;
[0054] e. Finally, dry the reaction product B at a temperature of 50°C to obtain the final product, namely the magnetic extreme pressure antiwear agent;
[0055] An energy-saving and environment-friendly engine oil utilizing the above-mentioned magnetic extreme-pressure anti-wear agent, specifically comp...
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