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Preparation method and application of a kind of biochar-based composition

A technology of biochar and composition, applied in the application, fertilizer mixture, chemical instrument and method, etc., can solve the problems of unstable repair effect and short duration, achieve no secondary pollution, low cost, and high efficiency. Yield effect

Active Publication Date: 2020-05-12
INST OF AGRI RESOURCES & ENVIRONMENT GUANGDONG ACADEMY OF AGRI SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In view of this, the present invention provides a preparation method and application of a biochar-based composition, which is used to solve the technical defects in the prior art of remediating heavy metal pollution, such as unstable remediation effect and short duration

Method used

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  • Preparation method and application of a kind of biochar-based composition
  • Preparation method and application of a kind of biochar-based composition
  • Preparation method and application of a kind of biochar-based composition

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Weigh 1000g of sawdust, dry and pulverize it until the particle size is less than 25mm, put it into an atmosphere box furnace, pump it into a vacuum and feed nitrogen as a protective gas, raise the temperature to 220°C at a rate of 6°C / min, stay for 30min, and then After heating up to 550°C / min, keep it warm for 3 hours, pass through a 20-mesh sieve after grinding, soak in 1mol / L hydrochloric acid for 3 hours, wash and dry to obtain wood chip biochar, which is the first intermediate product 1.

[0024] Weigh 100 g of alkali-making waste residue, dry and pulverize it, and pass through a 60-mesh sieve to obtain the second intermediate product 1.

[0025] Mix 250g of the first intermediate product 1 with 50g of the second intermediate product 1, pass through a 100-mesh sieve after drying, and obtain the product 1.

Embodiment 2

[0027] Weigh 1000g of rice husk, dry and pulverize until the particle size is less than 10mm, put it into a vacuum tube furnace, and after vacuuming, feed nitrogen as a protective gas, raise the temperature to 250°C at 8°C / min, stay for 25min, and then heat it up at 3°C / min. Min heat up to 550°C, keep it warm for 2 hours, grind through a 100-mesh sieve, soak in 3mol / L hydrochloric acid for 1 hour, wash and dry to obtain chaff biochar, which is the first intermediate product 2.

[0028] Weigh 100g of lime, dry and pulverize it, and pass through a 60-mesh sieve to obtain the second intermediate product 2.

[0029] Mix 300g of the first intermediate product 2 with 30g of the second intermediate product 2, pass through an 80-mesh sieve after drying, and obtain the product 2.

Embodiment 3

[0031] Weigh 1000g of corn stalks, dry and pulverize them until the particle size is less than 10mm, put them into an atmosphere box furnace, vacuumize and feed nitrogen as a protective gas, raise the temperature to 260°C at 10°C / min, stay for 45min, and then heat up to 260°C at 2°C / min After heating up to 750°C, keep it warm for 1 hour, grind it through a 100-mesh sieve, soak it in 2mol / L hydrochloric acid for 2 hours, wash and dry it to prepare corn straw biochar, which is the first intermediate product 3.

[0032] Weigh 100 g of alkali-making waste residue, dry and pulverize it through a 60-mesh sieve to obtain the second intermediate product 3.

[0033] Mix 200g of the first intermediate product 3 with 60g of the second intermediate product 3, pass through an 80-mesh sieve after drying, and obtain the product 3.

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Abstract

The invention belongs to the field of soil remediation, and particularly relates to a preparation method and application of a biological charcoal-based composition. The preparation method of the biological charcoal-based composition comprises the steps that 1, agriculture and forestry wastes are subjected to pyrolysis carbonization, cooled to room temperature, activated and then crushed, and a first product is prepared; 2, an alkaline regulating agent is dried and then crushed, and a second product is prepared; 3, the first product and the second product are mixed, dried and then crushed, and the biological charcoal-based composition is obtained. The invention further provides application of the biological charcoal-based composition in soil improvement. According to the technical scheme, experimental determination shows that the content of heavy metals in soil can be effectively decreased, the pH of the soil is improved, and the yield of crops planted in the soil is increased; the problem that in the prior art, the technical defects that the remediation effect is unstable, and the duration time is short mainly exist in heavy metal contamination remediation is solved; meanwhile, the advantages of being low in cost and convenient and easy to obtain and not causing secondary contamination are achieved.

Description

technical field [0001] The invention belongs to the field of soil treatment, and in particular relates to a preparation method and application of a biochar-based composition. Background technique [0002] With the rapid development of industrialization, urbanization and intensive agriculture, the problem of soil environmental pollution in my country is becoming more and more serious, among which heavy metals and organic pollutants are typical representatives. The 2014 "National Soil Pollution Survey Bulletin" revealed that my country's soil environment is worrying, manifested in the deterioration of the soil environment quality of cultivated land and a decreasing trend, and the soil pollution of industrial and mining wasteland is serious. The total soil pollution rate in the country is 16.1%, and the soil pollution in the south, especially in the Pearl River Delta region, is particularly prominent. In some cities in the Pearl River Delta, nearly 40% of the soil heavy metal ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K17/04C09K17/06C09K101/00C09K109/00
CPCC09K17/04C09K17/06C09K2101/00C09K2109/00
Inventor 李衍亮黄玉芬刘忠珍魏岚黄连喜徐培智黄庆许桂芝
Owner INST OF AGRI RESOURCES & ENVIRONMENT GUANGDONG ACADEMY OF AGRI SCI