Method for simultaneously separating rubidium and cesium from salt lake water
A technology for simultaneous separation and salt lake water, applied in chemical instruments and methods, water/sewage treatment, water treatment parameter control, etc., can solve the problems of lack of simple and feasible methods, achieve high selectivity, high separation efficiency, and simple operation Effect
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Embodiment 1
[0026] Dissolve 0.5g of the compound Calix[4]Bis(18Crown6) shown in structural formula I in 45.0mL of dichloromethane, mix uniformly to obtain a solution; add 4.5gSiO to this solution 2 -P Stir evenly, and use a rotary evaporator to evaporate dichloromethane under reduced pressure to volatilize the methylene chloride until the material is in a near-dry state, and then vacuum-dry the near-dry material at 55°C for 24 hours to obtain an adsorbent.
Embodiment 2
[0028] Dissolve 0.5g of the compound Calix[4]Bis(18Crown6) shown in structural formula I in 40.0mL of dichloromethane, mix well to obtain a solution; add 4.0g of SiO to this solution 2 -P Stir evenly, and use a rotary evaporator to evaporate dichloromethane under reduced pressure to volatilize the material to a near-dry state, and then vacuum-dry the near-dry material at 50°C for 24 hours to obtain an adsorbent.
Embodiment 3
[0030] Dissolve 0.5g of the compound Calix[4]Bis(18Crown6) shown in structural formula I in 50.0mL of dichloromethane, mix uniformly to obtain a solution; add 5.5gSiO to this solution 2 -P Stir evenly, and use a rotary evaporator to evaporate dichloromethane under reduced pressure to volatilize the methylene chloride until the material is in a near-dry state, and then vacuum-dry the near-dry material at 60°C for 24 hours to obtain an adsorbent.
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