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Tartary buckwheat rutin extracting method

An extraction method, the technology of tartary buckwheat rutin, applied in the field of tartary buckwheat rutin extraction, can solve the problems of high cost, viscous extract solution, starch gelatinization, etc., and achieve the effect of low cost and avoiding starch gelatinization

Active Publication Date: 2016-12-14
XICHANG COLLEGE +4
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the rutin used is mainly extracted from Sophora japonica (dried flower buds of Sophora japonica) by alkali extraction and acid precipitation. Due to the single source and difficulty in obtaining materials, the output of rutin is greatly limited, resulting in a shortage of rutin. unable to meet social needs
Tartary buckwheat is the only food crop with high rutin content that has been found so far. The whole tartary buckwheat grain contains tartary buckwheat shell, seed coat (the main source of tartary buckwheat bran, the part with the highest rutin content), tartary buckwheat core (starch source The main part), wherein the rutin content in the seed coat is the highest, and its content exceeds 5%, but it is not suitable for the traditional method of alkali extraction and acid precipitation. The main reason is that tartary buckwheat bran contains starch. Starch gelatinization is caused, and the entire extract is viscous, which makes it impossible to separate and purify rutin at a low cost in the later stage. If organic solvent is used for extraction, the cost is too high

Method used

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  • Tartary buckwheat rutin extracting method
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  • Tartary buckwheat rutin extracting method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Select whole tartary buckwheat seeds and clean them, then put the cleaned tartary buckwheat seeds into clean water, soak for 2-24 hours at 10-50°C, drain the tartary buckwheat seeds after soaking, and then drain The tartary buckwheat seeds with moisture are dried in an environment with a temperature of 105° C., and the drying time is 20-200 minutes. Then, the dried tartary buckwheat seeds are divided into 16 groups, and the weight of each group of tartary buckwheat seeds is 100 g. Add different weights of lime water with a pH value of 8 to 9 to each group, perform ultrasonic constant temperature leaching at 80°C for different periods of time, and then suction filter to determine the rutin extraction yield. Refer to the percentage that the rutin powder finally obtained accounts for the total rutin content of tartary buckwheat seeds, and the reaction conditions and measurement results of each group are as shown in Table 1 below:

[0028] Table 1

[0029]

[0030]

Embodiment 2

[0032] Select whole tartary buckwheat seeds and clean them, then put the cleaned tartary buckwheat seeds into clean water, soak for 2-24 hours at 10-50°C, drain the tartary buckwheat seeds after soaking, and then drain The tartary buckwheat seeds with moisture are dried in an environment with a temperature of 105° C., and the drying time is 20-200 minutes. Then, the dried tartary buckwheat seeds are divided into 16 groups, and the weight of each group of tartary buckwheat seeds is 100 g. Add different weights of lime water with a pH value of 8 to 9 in each group, suction filter after 20 minutes of ultrasonic constant temperature leaching under different temperature conditions, and measure the extraction yield of rutin. The extraction yield of rutin is Refer to the percentage that the rutin powder finally obtained accounts for the total rutin content of tartary buckwheat seeds, and the reaction conditions and measurement results of each group are shown in Table 2 below:

[0033...

Embodiment 3

[0038] Select whole tartary buckwheat seeds and clean them, then put the cleaned tartary buckwheat seeds into clean water, soak for 2-24 hours at 10-50°C, drain the tartary buckwheat seeds after soaking, and then drain The tartary buckwheat seeds with moisture are dried in an environment with a temperature of 105° C., and the drying time is 20-200 minutes. Then, the dried tartary buckwheat seeds are divided into 16 groups, and the weight of each group of tartary buckwheat seeds is 100 g. Add 1000g of lime water with a pH value of 8 to 9 to each group, carry out ultrasonic constant temperature leaching for different times under different leaching temperature conditions, and then suction filter to measure the leaching yield of rutin. Yield refers to the percentage of rutin powder finally obtained in the total rutin content of tartary buckwheat seeds. The reaction conditions and measurement results of each group are shown in Table 3 below:

[0039] table 3

[0040]

[0041] ...

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Abstract

The invention discloses a tartary buckwheat rutin extracting method which is low in cost and high in extracting rate. The method comprises the steps that whole-grain tartary buckwheat seeds are adopted as raw materials, the tartary buckwheat seeds are washed clean and then placed in clear water to be soaked for 2h to 24 h at the temperature of 10 DEG C-50 DEG C, and water of the tartary buckwheat seeds is leached; the tartary buckwheat seeds are subjected to drying treatment and then placed in a container containing an alkaline solution to be subjected to ultrasonic constant-temperature extracting, so that rutin contained in seed coats of the tartary buckwheat seeds is dispersed inwards and outwards. Due to the fact that starch is wrapped by the seed coats and tartary buckwheat shells, the starch in tartary buckwheat can be prevented from entering an extracting solution when the whole-grain tartary buckwheat is extracted through the alkaline solution, then starch pasting can be prevented, the tartary buckwheat rutin can be easily separated out only by conducting standing on a tartary buckwheat extracted solution for a period of time, and the cost is very low. Meanwhile, the tartary buckwheat rutin is extracted from the tartary buckwheat seed coats in the method, and therefore the more tartary buckwheat rutin can be extracted. The method is suitable for being applied and popularized in the technical field of tartary buckwheat processing.

Description

technical field [0001] The invention relates to the technical field of tartary buckwheat processing, in particular to a method for extracting tartary buckwheat rutin. Background technique [0002] Rutin, synonymous with rutin, is yellow or yellow-green powder, or very fine needle-like crystals; odorless, tasteless, and gradually darkens in the air: heated to 185-192 ° C to turn into a brown jelly. Rutin is a vitamin drug, which can reduce the permeability and fragility of capillaries, maintain and restore the normal elasticity of capillaries. It is used to prevent and treat hypertensive cerebral hemorrhage; diabetic retinal hemorrhage and hemorrhagic purpura, etc. It is also used as food antioxidant and pigment. Rutin is also the main raw material for the synthesis of troxerutin. Troxerutin is a cardiovascular and cerebrovascular medicine, which can effectively inhibit the aggregation of platelets and prevent thrombosis. Therefore, rutin has high medical value. At present...

Claims

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Application Information

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IPC IPC(8): C07H17/07C07H1/08
CPCC07H1/08C07H17/07
Inventor 巩发永李静杨建平向丹肖诗明徐凤娟邓桃
Owner XICHANG COLLEGE