Unlock instant, AI-driven research and patent intelligence for your innovation.

A method for fractional extraction of fulvic acid xad resin from sludge and straw mixed compost

A technology of fractional extraction and fulvic acid, applied in the direction of organic chemistry, etc., can solve the problems of low content of fulvic acid and complex components

Inactive Publication Date: 2017-10-31
CHINESE RES ACAD OF ENVIRONMENTAL SCI
View PDF5 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the finished compost system includes both minerals in sludge and animal and plant residues. Its composition is quite complex and the content of fulvic acid in the finished compost is very small. Certain technical methods are required to extract fulvic acid from the finished compost. out, further enrichment and fractionation of fulvic acid

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0092] In this example, the compost fulvic acid subcomponents of sludge and straw in a certain sewage treatment plant are graded and extracted, and the treated sludge of a certain sewage treatment plant is firstly selected (discharged up to the standard, and the water content, N, P, Heavy metal content, record data), and mix it with straw with a length between 3cm -5cm, including the following steps:

[0093] The preparation process of sludge and straw mixed compost is as follows:

[0094] 1) Select the sludge that meets the standard after treatment in the sewage treatment plant, and monitor the water content, N, P, heavy metal and organic matter content of the sludge; cut the plant straw so that the length of the straw is 3cm;

[0095] 2) According to the weight ratio of 1:1.5, put the sludge and straw in a commercially available composting reactor, stir and stir well, and ensure that the initial moisture content is 50-70%;

[0096] 3) In the composting stage, the mixed samp...

Embodiment 2

[0136] A method for fractional extraction of fulvic acid XAD resin in sludge and straw mixed compost, said extraction method comprising the following steps:

[0137] The preparation process of sludge and straw mixed compost is as follows:

[0138] 1) Select the sludge that meets the standard after treatment in the sewage treatment plant, and monitor the water content, N, P, heavy metal and organic matter content of the sludge; cut the plant straw so that the length of the straw is 3cm -5cm;

[0139] 2) According to the weight ratio of 1: (1-2), put the sludge and straw in a commercially available composting reactor, stir and turn evenly to ensure that the initial moisture content is 50%-70%, if the moisture content is lower than 50% %, carry out water treatment; if the water content is higher than 70%, carry out drying treatment;

[0140] 3) In the composting stage, the mixed sample after composting is obtained. The time period is 100-130 days. During the composting period, t...

Embodiment 3

[0168] A method for fractional extraction of fulvic acid XAD resin in sludge and straw mixed compost, said extraction method comprising the following steps:

[0169] The preparation process of sludge and straw mixed compost is as follows:

[0170] 1) Select the sludge that meets the standard after treatment in the sewage treatment plant, and monitor the water content of the sludge, the content of N, P, heavy metals and organic matter; cut the plant straw so that the length of the straw is 5cm;

[0171] 2) According to the weight ratio of 1:1, put the sludge and straw in a commercially available composting reactor, stir and turn evenly, and ensure that the initial moisture content is 50%-70%;

[0172] 3) In the composting stage, the mixed sample after composting is obtained. The time period is 130 days. During the composting period, the temperature of the compost is measured every 7 hours every day. Every 8 days, the sludge and straw are stirred and sampled, and their water con...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
lengthaaaaaaaaaa
lengthaaaaaaaaaa
lengthaaaaaaaaaa
Login to View More

Abstract

The invention belongs to the technical field of separation and extraction of organic matter, and discloses a method for fractional extraction of fulvic acid XAD resin in sludge and straw mixed compost. The method comprises the following steps: a. Separation and extraction process of fulvic acid in mixed compost of sludge and straw: extracting fulvic acid in a sample of mixed compost of sludge and straw, removing silicon, removing salt, and drying to obtain a fulvic acid sample; b. Fractional extraction process of fulvic acid in mixed compost of sludge and straw: using the adsorption performance of XAD-4 resin and XAD-8 resin mixed adsorption enrichment column, use KNO3 or NaNO3 eluent with gradient pH value to leach Wash the adsorption enrichment column to obtain the corresponding fulvic acid subcomponents at different pH values; c, the purification process of the fulvic acid subcomponent solution samples. The invention provides a new method for the separation and fractional extraction of fulvic acid subcomponents in sludge and straw mixed compost.

Description

technical field [0001] The invention belongs to the technical field of separation and extraction of organic matter, and relates to a method for fractional extraction of fulvic acid XAD resin in sludge and straw mixed compost. Background technique [0002] The composting of sludge and straw can effectively realize waste reuse and resource utilization while realizing harmless and resourceful solid waste. The high-temperature aerobic composting technology in the composting process of sludge and straw uses aerobic bacteria and oxygen to ferment sludge and straw at high temperature, and gradually degrades unstable organic matter into compost products with stable properties and harmless to crops. [0003] Fulvic acid (FA) exists in every link of the ecosystem and is an important participant in the energy cycle carrier and material cycle in the ecosystem. The fulvic acid rich in the finished compost of sludge and straw plays a very important role in the application of nutrients an...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C08H99/00C07G99/00
CPCC08H6/00C08H99/00C07G99/00
Inventor 宋凡浩白英臣吴丰昌陈曲冯伟莹刘沙沙
Owner CHINESE RES ACAD OF ENVIRONMENTAL SCI