A kind of nepetalactone microcapsule, its preparation method and its application in the preparation of mosquito repellent products
A technology of nepetalactone and ester microcapsules, applied in the field of daily chemicals, can solve the problems of application limitation, strong volatility effect of pseudo nepetalactone, short-lived, strong volatility, etc. The effect of high encapsulation rate
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Embodiment 1
[0055] Dissolve 40g of gelatin in 200mL of deionized water, 80g of porous starch in 400mL of deionized water, heat and stir at 70°C until clear and transparent; dissolve 4g of nepetalactone in 50mL of absolute ethanol, preheat, Then the solution was added dropwise into the porous starch solution, and continuously stirred for 1 h, then added into the gelatin solution and continued to stir for 2 h, and finally a coarse emulsion containing nepetalactone microcapsules was obtained. The above emulsion is spray-dried, the conditions are: the feed flow rate is 60ml / min, and the drying air flow rate is 75m 3 / h, the hot air inlet temperature is 200°C, and the outlet temperature is 60°C.
Embodiment 2
[0057] Dissolve 60g of gelatin in 300mL of deionized water, 60g of porous starch in 300mL of deionized water, heat and stir at 80°C until clear and transparent; dissolve 10g of nepetalactone in 100mL of absolute ethanol, preheat, Then add the solution dropwise into the porous starch solution, and keep stirring for 2 hours, then add the gelatin solution and continue stirring for 1.5 hours, and finally obtain a coarse emulsion containing nepetalactone microcapsules. The above emulsion is spray-dried, the conditions are: the feed flow rate is 70ml / min, and the drying air flow rate is 70m 3 / h, the hot air inlet temperature is 190°C, and the outlet temperature is 65°C.
Embodiment 3
[0059] Dissolve 80g of gelatin in 400mL of deionized water, 40g of porous starch in 200mL of deionized water, heat and stir at 75°C until clear and transparent; dissolve 7g of nepetalactone in 75mL of absolute ethanol, preheat, Then the solution was added dropwise into the porous starch solution, and kept stirring for 2.5 hours, then added the gelatin solution and continued to stir for 3 hours, and finally obtained a coarse emulsion containing nepetalactone microcapsules. The above emulsion is spray-dried, the conditions are: the feed flow rate is 70ml / min, and the drying air flow rate is 80m 3 / h, the hot air inlet temperature is 180°C, and the outlet temperature is 70°C.
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