Casting epoxy resin composition for part repair
A technology of epoxy resin and composition, which is applied in the preparation of cast epoxy resin composition and the synthesis process of epoxy resin, can solve the problem of low thermal deformation temperature of cured product, affecting the overall appearance of the product, and inconsistency with production efficiency, etc. problem, to achieve the effect of fast curing speed, maintaining processability, reducing curing shrinkage and thermal stress
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Embodiment 1
[0025] Step 1) Preparation of resin: Preheat bisphenol A epoxy resin E-55 to 60-65°C, preheat polyurethane modified epoxy resin to 75-80°C; then preheat 100 parts of bisphenol A Type epoxy resin E-55, 30 parts of polyurethane modified epoxy resin and 20 parts of epoxy diluent polypropylene glycol diglycidyl ether were added to the reaction kettle in sequence, and the stirring was started to keep the temperature in the tank at 50-70°C. The speed is less than 100rpm, stir for 30-60min and then cool to 30-40°C; add 2 parts of defoamer, continue stirring for 20-40min, and finally carry out vacuum defoaming, defoaming while stirring for 20-40min, then stop stirring to obtain resin mixture liquid;
[0026] Step 2) Preparation of curing agent: In another reaction kettle, add 80 parts of aliphatic amine tetraethylenepentamine in parts by weight, start stirring and keep the temperature in the tank at about 25-40°C, and then add 10 parts in sequence Alicyclic amine 1,3-bis(aminomethyl)...
Embodiment 2
[0030] Step 1) Preparation of resin: Preheat bisphenol A epoxy resin E-55 to 60-65°C, preheat polyurethane modified epoxy resin to 75-80°C; then preheat 100 parts of bisphenol A Type epoxy resin E-55, 20 parts of polyurethane modified epoxy resin and 15 parts of epoxy diluent polypropylene glycol diglycidyl ether were added to the reaction kettle in sequence, and the stirring was started to keep the temperature in the tank at 50-70°C. The speed is less than 100rpm, stir for 30-60min and then cool to 30-40°C; add 1 part of defoamer, continue stirring for 20-40min, and finally carry out vacuum defoaming, defoaming while stirring for 20-40min, then stop stirring to obtain resin mixture liquid;
[0031] Step 2) Preparation of curing agent: In another reaction kettle, add 70 parts of aliphatic amine tetraethylenepentamine, start stirring and keep the temperature in the tank at about 25-40°C, then add 10 parts of alicyclic amine 1 in sequence, 3-bis(aminomethyl)cyclohexane, 10 part...
Embodiment 3
[0035] Step 1) Preheat bisphenol A type epoxy resin E-51 to 60-65°C, preheat dimer acid modified epoxy resin to 75-80°C; then preheat 100 parts of bisphenol A type Epoxy resin E-51, 15 parts of dimer acid-modified epoxy resin and 15 parts of diluent butanediol diglycidyl ether were added to the reaction kettle in sequence, and the stirring was started to keep the temperature in the tank at 50-70°C. The speed is less than 100rpm, stir for 30-60min and then cool to 30-40°C; add 0.5 parts of defoamer, continue stirring for 20-40min, and finally carry out vacuum defoaming, stirring while defoaming for 20-40min, then stop stirring to obtain resin mixture liquid;
[0036] Step 2) Preparation of curing agent: In another reaction kettle, add 60 parts of aliphatic amine triethylenetetramine and 10 parts of polyetheramine D-400, start stirring and keep the temperature in the tank at about 25-40 °C, and then sequentially Add 15 parts of the cycloaliphatic amine 1,3-bis(aminomethyl)cyclohe...
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