Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Water-soluble degradable quenching medium

A quenching agent, water-soluble technology, applied in the direction of quenching agent, heat treatment equipment, manufacturing tools, etc., can solve the problems of clean production environment, high corrosiveness of quenching agent, deformation of workpiece, etc., to achieve high practical value, low environmental pollution, Avoid cracking effects

Inactive Publication Date: 2017-03-22
HENAN TIMECLOUD COMM TECH CO LTD
View PDF0 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantage is that the workpiece is prone to "soft spots" during the cooling process, and in the martensitic transformation temperature zone, due to too fast cooling, it is easy to generate a large internal stress, resulting in deformation or even cracking of the workpiece
Part of the water-based quenching agent adds an appropriate amount of salt and alkali to the water, so that after the high-temperature workpiece is immersed in the cooling medium, crystals of salt and alkali can be precipitated in the steam film stage and burst immediately, thereby destroying the steam film and shattering the surface oxidation of the workpiece. Quenching agent can improve the cooling capacity of the medium in the high temperature area, but this kind of quenching agent is highly corrosive and affects the cleanliness of the production environment

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] A water-soluble degradable quenching agent, which is composed of the following raw materials in parts by weight: 2 parts of methanol, 4 parts of rhamnolipid, 6 parts of acetic acid, 2 parts of butyl hydroxyanisole, 8 parts of rapeseed oil, cyclodextrose 11 parts of essence, 6 parts of pine oil, 15 parts of acrylic acid, 7 parts of sucrose, 0.5 parts of 2-thione-trimethylol benzothiazoline, and 10 parts of shell powder.

[0017] A kind of preparation method of water-soluble degradable quenching agent, concrete steps are:

[0018] First, dissolve acetic acid, butyl hydroxyanisole, and pine oil in methanol to obtain a mixed solution, then add water 1 times the volume of the mixed solution and transfer it to a reactor. The reaction conditions are 115°C, 900r / min, 5MPa. The time is 30min. After the reaction is over, the temperature drops to 64.3°C, add rhamnolipid, rapeseed oil, cyclodextrin, sucrose, stir for 10min and then let it stand; then carry out centrifugation, the c...

Embodiment 2

[0020] A water-soluble degradable quenching agent, which consists of the following raw materials in parts by weight: 2 parts of methanol, 5 parts of rhamnolipid, 8 parts of acetic acid, 2 parts of butyl hydroxyanisole, 8 parts of rapeseed oil, cyclodextrose 14 parts of essence, 8 parts of pine oil, 18 parts of acrylic acid, 7 parts of sucrose, 0.6 parts of 2-thione-trimethylol benzothiazoline, 14 parts of shell powder.

[0021] A kind of preparation method of water-soluble degradable quenching agent, concrete steps are:

[0022] First, dissolve acetic acid, butyl hydroxyanisole, and pine oil in methanol to obtain a mixed solution, then add water 1 times the volume of the mixed solution and transfer it to a reactor. The reaction conditions are 115°C, 900r / min, 5MPa. The time is 30min. After the reaction is over, the temperature drops to 64.3°C, add rhamnolipid, rapeseed oil, cyclodextrin, sucrose, stir for 10min and then let it stand; then carry out centrifugation, the centrifu...

Embodiment 3

[0024] A water-soluble degradable quenching agent, which is composed of the following raw materials in parts by weight: 4 parts of methanol, 6 parts of rhamnolipid, 9 parts of acetic acid, 3 parts of butyl hydroxyanisole, 10 parts of rapeseed oil, cyclodextrose 15 parts of essence, 9 parts of pine oil, 20 parts of acrylic acid, 8 parts of sucrose, 0.7 parts of 2-thione-trimethylol benzothiazoline, 16 parts of shell powder.

[0025] A kind of preparation method of water-soluble degradable quenching agent, concrete steps are:

[0026] First, dissolve acetic acid, butyl hydroxyanisole, and pine oil in methanol to obtain a mixed solution, then add water that is 1 times the volume of the mixed solution and transfer it to a reactor. The reaction conditions are 118°C, 950r / min, and 7MPa. The time is 35min. After the reaction is over, the temperature drops to 64.3°C, add rhamnolipid, rapeseed oil, cyclodextrin, sucrose, stir for 10min and then let stand; then centrifuge, the centrifug...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a water-soluble degradable quenching medium. The water-soluble degradable quenching medium is composed of, by weight, 2-6 parts of methyl alcohol, 4-8 parts of rhamnolipid, 6-10 parts of acetic acid, 2-4 parts of butylated hydroxyanisole, 8-12 parts of rapeseed oil, 11-17 parts of cyclodextrin, 6-10 parts of pine oil, 15-25 parts of acrylic acid, 7-8 parts of cane sugar, 0.5-0.8 part of 2-thioketone-tris(hydroxymethyl) benzisothiazolin and 10-20 parts of shell powder. Firstly, the acetic acid, the butylated hydroxyanisole and the pine oil are dissolved in the methyl alcohol, and a mixed solution is obtained; then, water is added, and the mixture is transferred into a reaction kettle; after the reaction ends, cooling is conducted, the rhamnolipid, the rapeseed oil, the cyclodextrin and the cane sugar are added, and the mixture stands after being stirred for 10 min; then, centrifugation is conducted, supernate is taken after centrifugation, the acrylic acid, the 2-thioketone-tris(hydroxymethyl) benzisothiazolin and the shell powder are added, heating, heat preservation and cooling are conducted after the mixture is stirred to be uniform, sealing is conducted through paraffin, and the water-soluble degradable quenching medium is obtained. The prepared quenching medium has good water solubility, is ecologically degradable and is small in environment pollution.

Description

technical field [0001] The invention relates to the technical field of materials, in particular to a water-soluble degradable quenching agent. Background technique [0002] Quenching medium in heat treatment production directly affects the performance of parts after quenching, and is a key factor affecting product quality. Commonly used quenching media mainly include water, aqueous solution, oil, etc. Among them, quenching oil is very polluting to the environment, and it is easy to cause fire during quenching, so it is difficult to meet the requirements of safety and environmental protection. [0003] Water is a quenching medium with strong cooling capacity. It has wide sources, low price, stable composition and not easy to deteriorate. The disadvantage is that the workpiece is prone to "soft spots" during the cooling process, and in the martensitic transformation temperature zone, due to too fast cooling, it is easy to generate a large internal stress, resulting in deforma...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C21D1/58
CPCC21D1/58
Inventor 不公告发明人
Owner HENAN TIMECLOUD COMM TECH CO LTD
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products