Resin composition for forming cured film
A technology of resin composition and cured film, applied in the direction of coating, can solve the problems of complicated process and cost, and achieve the effect of excellent flexibility, excellent resistance and high hardness
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[0107] [Preparation method of composition]
[0108] The method for preparing the composition of the present invention is not particularly limited. As an example, the method of dissolving the component (A) in the solvent (D) and mixing the components (B) and (C) in an arbitrary order in a predetermined ratio in this solution to prepare a uniform solution . Moreover, the manufacturing method which further adds (E)-(I) component and other components as needed in the appropriate stage of this manufacturing method, and mixes it is mentioned. The cured film-forming resin composition in a solution state prepared in this way is preferably used after filtration using a filter having a pore diameter of about 0.2 μm or the like.
[0109] [Coated film and cured film]
[0110] Printing by using spin coating, flow coating, roll coating, slit coating, slit next spin coating, inkjet coating, screen printing, flexographic printing, gravure printing, offset printing, gravure offset printing,...
Embodiment 1
[0131] 41.5 g of CYCLOMER-P, 9.8 g of PET-30, 9.8 g of CYMEL303, 0.6 g of PERBUTYL L, 0.2 g of UPS, and 37.5 g of DEGEEA were charged in a 200 mL container. This was put into a stirring apparatus, and it stirred at 2,000 rpm for 10 minutes, and the composition (varnish) was produced.
Embodiment 2
[0133] 33.5 g of CYCLOMER-P, 11.8 g of PET-30, 11.8 g of CYMEL303, 0.5 g of PERBUTYL L, 0.2 g of UPS, and 42.2 g of DEGEEA were charged in a 200 mL container. This was put into a stirring apparatus, and it stirred at 2,000 rpm for 10 minutes, and the composition (varnish) was produced.
[0134] [2] Manufacture and evaluation of cured film
[0135] [2-1] Measurement of light transmittance
[0136] The varnishes of Examples 1 and 2 were respectively coated on quartz glass substrates by spin coating, and prebaked at 110° C. for 2 minutes. Next, post-baking was performed at 230° C. for 30 minutes to prepare a cured film with a thickness of 2 μm.
[0137] Then, the light transmittance in wavelength 400nm of each obtained cured film was measured. It should be noted that the light transmittance of the quartz glass substrate used was 93.8%.
[0138] [2-2] Evaluation of pencil hardness and adhesion
[0139] The varnishes of Examples 1 and 2 were respectively applied on glass subst...
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