A kind of preparation method of high hot pepper essence
A technology of chili extract and high spiciness, which is applied in the field of increasing the spiciness of chili extract and improving the quality of chili extract. It can solve problems such as affecting the use of chili extract, difficulty in meeting demand, and poor oil solubility, so as to achieve safe and pollution-free solvents. The effect of high consumption and cumbersome steps
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[0023] A preparation method of high-spicy capsicum extract, comprising the following steps:
[0024] 1) Add the crude pepper essence to the edible oil at a weight ratio of 1:2 to 1:5. The edible oil is vegetable oil or animal oil, preferably vegetable salad oil, and stir at a temperature of 40-45°C 30-60 minutes, keep warm and stand still, the standing temperature is 35-45°C, and the standing time is 4-6 hours. After the layers are separated, the upper mixture layer and the lower impurity layer are obtained, and the impurity layer is discarded;
[0025] 2) Add lower alcohol to the remaining mixture layer in step 1), the weight ratio of the added lower alcohol to the mixture layer is 1:3-1:5, the lower alcohol added in the present invention is methanol or ethanol, lower alcohol The purity of the mixture is 70% to 80%. Stir for a period of time and stand still. The stirring time is 30 to 60 minutes, the standing temperature is 35 to 45°C, and the standing time is 3 to 6 hours. ...
Embodiment 1
[0029] 1) Put 50 kg of capsicum essence with a spiciness of 14.72% into a stainless steel reaction kettle, add 150 kg of edible oil, and stir at 40°C for 40 minutes; after stopping the stirring, let it stand at 40°C for 4 hours, and divide into two layers, The upper layer is the edible oil layer, the lower layer is the impurity layer, and then the impurities in the lower layer are released.
[0030] 2) Continue to add 600kg of 70% methanol to the edible oil layer in the step 1), stir at 45°C for 30 minutes, and stand at 40°C for 3 hours, and divide it into two layers, the upper layer is an organic solvent layer, and the lower layer is Cooking oil layer. Collect the edible oil layer of upper floor organic solvent layer and lower layer respectively;
[0031] 3) Concentrate the upper organic solvent layer at a temperature of 60°C and a vacuum of -0.07 Mpa, and then deodorize it at a temperature of 60°C and a vacuum of -0.07 Mpa to obtain high-spicy pepper essence; the lower laye...
Embodiment 2
[0034] 1) Put 50 kg of crude capsicum essence with a spiciness of 14.72% into a stainless steel reaction kettle, add 200 kg of edible oil, and stir at 45°C for 50 minutes. After the stirring was stopped, it was left to stand at 45° C. for 5 hours and divided into two layers, the upper layer was an edible oil layer, and the lower layer was an impurity layer, and then the impurities in the lower layer were released.
[0035] 2) Continue to add 800 kg of 75% methanol to the edible oil layer in step 1), stir at 45°C for 50 minutes, and stand at 45°C for 5 hours, and divide it into two layers, the upper layer is an organic solvent layer, and the lower layer For edible oil layer. Collect the edible oil layer of upper floor organic solvent layer and lower layer respectively;
[0036] 3) Concentrate the upper organic solvent layer at a temperature of 65°C and a vacuum of -0.08 Mpa, and then deodorize it at a temperature of 60°C and a vacuum of -0.09 Mpa to obtain high-spicy pepper es...
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