Method for preparing water-soluble yellow fluorescent carbon quantum dot by taking bagasse as raw material
A technology of yellow fluorescence and carbon quantum dots, applied in fluorescence/phosphorescence, chemical instruments and methods, nanotechnology for materials and surface science, etc., can solve the unfavorable continuous and large-scale production of fluorescent carbon quantum dots, carbon quantum yield Low, non-renewable energy and other issues, to achieve the effect of abundant carbon sources, high quantum yield, and stable fluorescence
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Embodiment 1
[0030] 1) Pre-treatment of bagasse;
[0031] 2) Mix ultrapure water and glycerol in a volume ratio of 2:1 to obtain a mixed solution for subsequent use;
[0032] 3) adding the bagasse obtained from the pretreatment to the mixed solution obtained in the step 2), stirring; and placing it in a microwave environment, and performing microwave treatment to obtain a brown solution;
[0033] 4) filter the brown solution to obtain a filtrate;
[0034] 5) dialyzing the filtrate;
[0035] 6) Evaporating the dialysate under constant temperature conditions to obtain water-soluble yellow fluorescent carbon quantum dots.
[0036] In the preparation method of the water-soluble yellow fluorescent carbon quantum dots using bagasse as raw material, in the step 3), placing in a microwave environment and performing microwave treatment, specifically: placing in a reaction tube of a microwave synthesizer , and the temperature is 180°C, the reaction power is 200W, and the reaction time is 30min. ...
Embodiment 2
[0041] 1) Pre-treatment of bagasse;
[0042] 2) Mix ultrapure water and glycerol in a volume ratio of 3:1 to obtain a mixed solution for subsequent use;
[0043] 3) adding the bagasse obtained from the pretreatment to the mixed solution obtained in the step 2), stirring; and placing it in a microwave environment, and performing microwave treatment to obtain a brown solution;
[0044] 4) filter the brown solution to obtain a filtrate;
[0045] 5) dialyzing the filtrate;
[0046] 6) Evaporating the dialysate under constant temperature conditions to obtain water-soluble yellow fluorescent carbon quantum dots.
[0047] In the preparation method of the water-soluble yellow fluorescent carbon quantum dots using bagasse as raw material, in the step 3), placing in a microwave environment and performing microwave treatment, specifically: placing in a reaction tube of a microwave synthesizer , and the temperature is 180°C, the reaction power is 200W, and the reaction time is 30min. ...
Embodiment 3
[0052] 1) Pre-treatment of bagasse;
[0053] 2) Mix ultrapure water and glycerol in a volume ratio of 5:1 to obtain a mixed solution for subsequent use;
[0054] 3) adding the bagasse obtained from the pretreatment to the mixed solution obtained in the step 2), stirring; and placing it in a microwave environment, and performing microwave treatment to obtain a brown solution;
[0055] 4) filter the brown solution to obtain a filtrate;
[0056] 5) dialyzing the filtrate;
[0057] 6) Evaporating the dialysate under constant temperature conditions to obtain water-soluble yellow fluorescent carbon quantum dots.
[0058] In the preparation method of the water-soluble yellow fluorescent carbon quantum dots using bagasse as raw material, in the step 3), placing in a microwave environment and performing microwave treatment, specifically: placing in a reaction tube of a microwave synthesizer , and the temperature is 180°C, the reaction power is 200W, and the reaction time is 30min. ...
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