Low-dielectric-constant high-frequency glass ceramic LTCC material and preparation method thereof

A glass-ceramic, high-frequency technology, applied in glass manufacturing equipment, glass molding, manufacturing tools, etc., can solve the problems of large loss, achieve the effects of lower melting temperature, lower dielectric loss, and simple preparation process

Active Publication Date: 2017-05-17
NANJING INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention is that the present invention provides a low-dielectric and high-frequency glass-ceramic LTCC material for the technical problem of excessive loss of the existing glass-ceramic material system at high frequencies; further, the present invention provides a A method for preparing low-dielectric and high-frequency glass-ceramics LTCC materials, the method has simple preparation process and stable quality, can effectively control the precipitation of YAG phase, and obtain a series of glass-ceramics with dielectric constants from 5 to 9

Method used

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  • Low-dielectric-constant high-frequency glass ceramic LTCC material and preparation method thereof
  • Low-dielectric-constant high-frequency glass ceramic LTCC material and preparation method thereof
  • Low-dielectric-constant high-frequency glass ceramic LTCC material and preparation method thereof

Examples

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Embodiment 1

[0030] A low-dielectric and high-frequency glass-ceramic LTCC material, according to 1 in Table 1 # ~5 # The ingredients shown are equipped with mixed powder respectively, and 1 # mixed powder, 2 # mixed powder, 3 # powder mix, 4 # Mix powder and 5 # Mix the powder.

[0031] A method for preparing a low-dielectric and high-frequency glass-ceramic LTCC material, comprising the steps of:

[0032] The first step, ingredients: will 1 # The mixed powder is placed in a planetary ball mill for ball milling for 4 hours, and the speed of the planetary ball mill is 200rpm;

[0033] The second step is to prepare glass powder: the ball milled 1 # The mixed powder is placed in a high-temperature glass melting furnace, heated and melted, and the heating and melting process is as follows: heat up to 1400°C, keep warm for 4 hours, stir with a quartz glass rod every 1 hour; cool down after the melt is clarified, pour the melt Quenched in distilled water to obtain 1 # Glass powder; mi...

Embodiment 2

[0041] A low-dielectric and high-frequency glass-ceramic LTCC material, according to 1 in Table 1 # ~5 # The ingredients shown are equipped with mixed powder respectively, and 1 # mixed powder, 2 # mixed powder, 3 # powder mix, 4 # Mix powder and 5 # Mix the powder.

[0042] A method for preparing a low-dielectric and high-frequency glass-ceramic LTCC material, comprising the steps of:

[0043] The first step, ingredients: will 1 # The mixed powder was placed in a planetary ball mill for ball milling for 8 hours, and the speed of the planetary ball mill was 150rpm;

[0044] The second step is to prepare glass powder: the ball milled 1 # The mixed powder is placed in a high-temperature glass melting furnace, heated and melted. The heating and melting process is as follows: heat up to 1500°C, keep warm for 2 hours, and stir with a quartz glass rod every 1 hour; after the melt is clarified, cool down and pour the melt Quenched in distilled water to obtain 1 # Glass powd...

Embodiment 3

[0053] A low-dielectric and high-frequency glass-ceramic LTCC material, according to 1 in Table 1 # ~5 # The ingredients shown are equipped with mixed powder respectively, and 1 # mixed powder, 2 # mixed powder, 3 # powder mix, 4 # Mix powder and 5 # Mix the powder.

[0054] A method for preparing a low-dielectric and high-frequency glass-ceramic LTCC material, comprising the steps of:

[0055] The first step, ingredients: will 1 # The mixed powder was placed in a planetary ball mill for ball milling for 6 hours, and the speed of the planetary ball mill was 180rpm;

[0056] The second step is to prepare glass powder: the ball milled 1 # The mixed powder is placed in a high-temperature glass melting furnace, heated and melted, and the heating and melting process is as follows: heat up to 1450°C, keep warm for 3 hours, stir with a quartz glass rod every 1 hour; cool down after the melt is clarified, pour the melt Quenched in distilled water to obtain 1 # Glass powder; ...

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Abstract

The invention discloses a low-dielectric-constant high-frequency glass ceramic LTCC material and a preparation method thereof. The material comprises the following components: 40-54wt% of Y2O3, 32-38wt% of Al2O3, 4-5wt% of ZnO, 5-8wt% of B2O3, 3-5wt% of alkali metal oxide, and 2-4wt% of rare earth oxide. The low-dielectric high-frequency glass ceramic LTCC material and the preparation method thereof provided by the invention solve the technical problem of over-large loss of an existing glass ceramic material system under a high frequency, the preparation process is simple and stable in quality, a YAG phase can be effectively controlled to be precipitated, and a series of glass ceramics having dielectric constants ranging from 5 to 9 is obtained.

Description

technical field [0001] The invention relates to a low-dielectric and high-frequency glass-ceramic LTCC material and a preparation method thereof, belonging to the technical field of electronic ceramics and its preparation. Background technique [0002] With the continuous development of electronic information technology in the direction of high frequency and digitalization, the requirements for miniaturization, integration and modularization of components are becoming increasingly urgent. Low Temperature Co-fired Ceramics (LTCC) technology is Electrical, mechanical, thermal, process characteristics, and high reliability have become one of the main technologies for electronic device modularization. LTCC technology requires microwave dielectric ceramics to be co-fired with Ag and Cu internal electrodes with high conductivity and low melting point. Therefore, low-temperature sintering of microwave dielectric ceramic materials has become a research hotspot. Traditional ceramic ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C10/02C03C6/00C03C4/16C03B19/06
CPCC03B19/06C03C1/00C03C4/16C03C10/00
Inventor 吕学鹏张保森巴志新王章忠
Owner NANJING INST OF TECH
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