Aerogel-containing gypsum material and preparation method thereof

A technology of gypsum material and airgel, which is applied in the field of building materials, can solve the problems that airgel powder and mortar mixture are difficult to compound, airgel cannot be stored for a long time, and airgel is difficult to produce, so as to overcome airgel The effect of uneven dispersion, overcoming airgel dust flying, and simple preparation method

Active Publication Date: 2017-05-31
苏州同玄新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For example, CN102910870A provides a kind of nano-silicon airgel / vitrified microbead composite thermal insulation mortar, which is directly added to the mortar mixture by airgel powder, but it is difficult to compound the airgel powder and mortar mixture, and in the process Airgel powder will disperse into the surrounding environment
Another example, CN 105439505A reports a SiO 2 Airgel mortar and its preparation method, which is made of modified SiO by hydrophobic airgel and silane coupling agent 2 Airgel, and then mixed with mortar, but the airgel modified by this silane coupling agent is difficult to prepare, the cost is high, and the modified airgel cannot be stored for a long time
In addition, the performance of existing building materials mixed with airgel powder is limited compared with traditional building materials, and there are usually defects such as airgel is easy to separate from building materials, and the performance of each part is greatly different.

Method used

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  • Aerogel-containing gypsum material and preparation method thereof
  • Aerogel-containing gypsum material and preparation method thereof
  • Aerogel-containing gypsum material and preparation method thereof

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preparation example Construction

[0020] The preparation method of a kind of airgel-containing gypsum material provided by the embodiment of the present invention comprises:

[0021] Uniformly mix the airgel-containing paste, water, thickener and air-entraining agent to form an airgel aqueous dispersion in a uniformly distributed foam state;

[0022] Mix gypsum powder, retarder and water evenly to form a gypsum mixture with standard consistency;

[0023] uniformly mixing the gypsum mixture with the airgel aqueous dispersion to form an airgel-containing mixed slurry;

[0024] The airgel-containing mixed slurry is hardened and dried to obtain the airgel-containing gypsum material.

[0025] In some preferred embodiments, the mass ratio of the airgel aqueous dispersion to the gypsum mixture in the aforementioned airgel-containing mixed slurry is (0.1-60): (40-99.9), preferably (10-60 ): (40-90), especially preferably (30-50): (50-70).

[0026] In some preferred embodiments, the preparation method may also inclu...

Embodiment 1

[0057] Embodiment 1 The preparation method of a kind of airgel-containing gypsum material involved in this embodiment comprises:

[0058] The silica airgel powder, deionized water and polyoxyethylene dioleate are uniformly mixed to form an airgel-containing ointment, and the airgel powder is evenly distributed in the ointment. Further, the paste containing airgel includes 15wt% airgel powder, 82wt% water and 3wt% polyoxyethylene dioleate. Further, the thermal conductivity of the coating formed by the aerogel-containing paste in a dry state is 0.041 W / m·K. Among them, the density of silica airgel powder is 0.065g / ml, the particle size is 0.16μm, and the specific surface area is 1150m 2 / g, the thermal conductivity is 0.024W / m·k.

[0059] Mix the airgel-containing ointment, lignin fiber and deionized water, and then stir the above mixture until it is completely dispersed, then add sodium dodecylbenzenesulfonate to the above solution, and use high-speed stirring equipment to mi...

Embodiment 2

[0066] Embodiment 2 The preparation method of a kind of airgel-containing gypsum material involved in this embodiment includes:

[0067] Titanium dioxide airgel powder, deionized water and polyoxyethylene sorbitol lanolin oleic acid derivative are evenly mixed to form an airgel-containing ointment, and the airgel powder is evenly distributed in the ointment. Further, the airgel-containing ointment includes 30wt% titanium dioxide airgel powder, 65wt% water and 5wt% polyoxyethylene sorbitan lanolin oleic acid derivative. Further, the thermal conductivity of the coating formed by the aerogel-containing paste in a dry state is 0.021 W / m·k. Among them, the density of titanium dioxide airgel powder is 0.25g / ml, the particle size is 0.020mm, and the specific surface is 650m 2 / g, the thermal conductivity is 0.015W / m·k.

[0068] Mix the ointment containing airgel, polyethylene glycol and deionized water, and then stir the above mixture until it is completely dispersed, then add sodi...

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Abstract

The invention discloses an aerogel-containing gypsum material and a preparation method thereof. The preparation method comprises the steps: uniformly mixing aerogel-containing coating gypsum, water, a thickener and an air-entraining agent, so as to form a uniformly-distributed-foam-state aerogel aqueous dispersion; uniformly mixing gypsum powder, a setting retarder and water so as to form a gypsum mixture of a standard-consistency state; uniformly mixing the gypsum mixture and the aerogel aqueous dispersion, so as to form an aerogel-containing size mixture; subjecting the aerogel-containing size mixture to hardening and drying, thereby obtaining the aerogel-containing gypsum material. The preparation method of the aerogel-containing gypsum material, disclosed by the invention, is simple and is easy in condition control, the problems during the preparation of aerogel-containing building materials in the prior art that aerogel dust flies, aerogel dispersion is non-uniform, and the like are solved, the coefficient of thermal conductivity of gypsum products can be greatly reduced, and the water resistance of the gypsum products can also be effectively improved.

Description

technical field [0001] The invention relates to a gypsum material, in particular to an aerogel-containing gypsum material and a preparation method thereof, belonging to the field of building materials. Background technique [0002] Gypsum and its products have microporous structure and heating dehydration performance, so they have excellent heat insulation, sound insulation and fire resistance functions. Compared with cement products, gypsum products have obvious advantages and are typical green building materials, especially in recent years. The reuse of by-product gypsum has gained huge economic and social benefits. However, the water resistance and thermal insulation properties of gypsum generally restrict the further development of gypsum products. [0003] The process of using traditional methods to reduce the thermal conductivity of gypsum materials and improve the water resistance of gypsum products is more complicated and will have a greater impact on the comprehens...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B28/14C04B38/08C04B111/27
Inventor 王璇王玉琼周朝开
Owner 苏州同玄新材料有限公司
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