Conductive silver glue, preparation method and application thereof
A technology of conductive silver glue and silver powder, which is applied in the direction of conductive adhesives, adhesives, epoxy resin glue, etc., can solve the problems of reducing bond strength and operating performance, poor storage and transportation performance, and increasing the viscosity of conductive adhesives, etc., to achieve Improve handling performance, improve electrical conductivity, and promote the effect of dispersion
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Embodiment 1
[0051] A conductive silver glue, comprising the following components by weight:
[0052] Ionic liquids ([BMIM][BF 4 ]) 1 serving
[0053] Silver powder (1~8μm) 80 parts
[0054] Epoxy resin (bisphenol A epoxy resin 828E) 16 parts
[0055] Curing agent (dicyandiamide) 1 part
[0056] Accelerator (1-cyanoethyl-2-ethyl-4-methylimidazole) 0.1 part
[0057] Coupling agent (KH560) 0.1 part
[0058] Diluent (1,4-butanediol diglycidyl ether) 1.75 parts
[0059] Anti-precipitation agent (fumed silica) 0.05 part;
[0060] Preparation:
[0061] Fill the ionic liquid into the epoxy resin according to the formula, stir and defoaming, so that the ionic liquid is fully dispersed, and the first basic resin with uniform components is prepared; diluent, anti-precipitation agent, coupling agent, curing agent, accelerator The silver powder is added to the first base resin according to the formula, and after mixing, it is ground evenly with a three-roll mill, mixed and defoamed to make a s...
Embodiment 2
[0073] The difference from Example 1 is that the conductive silver glue includes the following components in parts by weight:
[0074] Ionic liquids ([HEMIM][BF 4 ]) 1 serving
[0075] Silver powder (1~10μm) 80 parts
[0076] Epoxy resin (bisphenol A epoxy resin 828E) 16 parts
[0077] Curing agent (dicyandiamide) 1 part
[0078] Accelerator (1-cyanoethyl-2-ethyl-4-methylimidazole) 0.1 part
[0079] Coupling agent (KH560) 0.1 part
[0080] Diluent (1,4-butanediol diglycidyl ether) 1.75 parts
[0081] Anti-precipitation agent (fumed silica) 0.05 part;
Embodiment 3
[0083] The difference from Example 1 is that the conductive silver glue includes the following components in parts by weight:
[0084] Ionic liquid ([BMIM][DCA]) 1 part;
[0085] 80 parts of silver powder (3~6μm);
[0086] Epoxy resin (bisphenol A epoxy resin 828E) 16 parts
[0087] Curing agent (dicyandiamide) 1 part
[0088] Accelerator (1-cyanoethyl-2-ethyl-4-methylimidazole) 0.1 part
[0089] Coupling agent (KH560) 0.1 part
[0090] Diluent (1,4-butanediol diglycidyl ether) 1.75 parts
[0091] Anti-precipitation agent (fumed silica) 0.05 part;
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