Silicon dioxide coating resisting to high temperature and corrosion and preparation method and application thereof

A silicon dioxide and corrosion-resistant technology, applied in coatings, metal material coating processes, liquid chemical plating, etc., can solve problems such as being easily affected by water vapor in the air, poor hydrophobic performance, and unfavorable industrial production , to achieve the effect of ensuring long-term safe and stable operation, ensuring service life and low investment cost

Active Publication Date: 2017-06-23
哈尔滨金氙科技有限公司
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Problems solved by technology

[0009] The present invention aims to solve the technical problems that the current preparation method of silica coating generally needs to be carried out under high temperature conditions, which is not conducive to industrial production and generally has poor hydrophobic performance, is easily affected by water vapor in the air, and has a short service life; and Provided is a high temperature and corrosion resistant silicon dioxide coating and its preparation method and application

Method used

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  • Silicon dioxide coating resisting to high temperature and corrosion and preparation method and application thereof
  • Silicon dioxide coating resisting to high temperature and corrosion and preparation method and application thereof
  • Silicon dioxide coating resisting to high temperature and corrosion and preparation method and application thereof

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specific Embodiment approach 1

[0033] Specific embodiment one: the preparation method of the high-temperature and corrosion-resistant silicon dioxide coating of this embodiment is carried out according to the following steps:

[0034] Step 1. Weigh the raw materials according to the molar ratio of ethyl orthosilicate, absolute ethanol and deionized water as 15:21:81,

[0035] Then dehydrated ethanol was divided into two equal parts, wherein a part of dehydrated ethanol and ethyl orthosilicate were mixed and stirred for 20 minutes to obtain solution A,

[0036] Another part of absolute ethanol and deionized water was mixed and stirred for 20 minutes, then fluorosilane coupling agent was added dropwise to obtain solution B, and then solution A and solution B were mixed and stirred for 30 minutes in a water bath at 45°C under condensing and reflux conditions, and continued to stir At the same time, in step 1, add 3 drops of fluorosilane coupling agent per 2 g of 65% (mass) nitric acid, slowly drop N,N-dimethyl...

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Abstract

The invention discloses a silicon dioxide coating resisting to a high temperature and corrosion and a preparation method and application thereof, and belongs to the technical field of silicon dioxide coatings. The silicon dioxide coating resisting to the high temperature and corrosion and the preparation method and application thereof solve the technical problems that current preparation of silicon dioxide coatings is usually conducted under the condition of a high temperature, industrial production is thus not facilitated, generally the hydrophobic performance is poor, the coatings are easily affected by steam in air, and the service life is short. The preparation method comprises the steps that absolute ethyl alcohol is equally divided into two parts, one part of absolute ethyl alcohol and tetraethoxysilane are mixed and stirred to prepare a solution A, the other part of absolute ethyl alcohol and deionized water are mixed and stirred and then fluorosilane coupling agents are added dropwise to prepare a solution B, the solution A and the solution B are mixed and stirred under the conditions of heating in a water bath and reflux condensation, N,N-dimethyl formamide is slowly added dropwise, then nitric acid is added and stirred for reaction to prepare a glue solution, and a silicon steel sheet with an oxidation film removed is subjected to dipping and pulling through the glue solution and then subjected to secondary thermal treatment. The silicon dioxide coating resisting to the high temperature and corrosion is used as a turbine blade surface wear-resisting coating.

Description

technical field [0001] The invention belongs to the technical field of silicon dioxide coatings; in particular, it relates to a high-temperature and corrosion-resistant silicon dioxide coating and its preparation method and application; the product of the invention is used as fan blades, water turbine blades, and the like. Background technique [0002] Cracks in turbine blades seriously threaten the safe operation of the unit and reduce economic benefits. Blade cracks are fatigue cracks, which are mainly caused by alternating stress. If the blade cracks are found during the inspection, they generally need to be repaired. Cracked blades tend to have a shorter service life after repair welding, especially in machine pits. Blade cracks not only reduce economic benefits due to downtime and reduce power generation, but also directly affect the safe operation of the unit. The emergence of the serious problem of frequent blade cracking of large and medium-sized water turbines in...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C18/12
CPCC23C18/1212
Inventor 翁凌张迎春张笑瑞刘立柱
Owner 哈尔滨金氙科技有限公司
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